di-18(O)-methyl phenyl sulfone

Base Information

• Chemical Name: di-18(O)-methyl phenyl sulfone
• CAS No.: 454705-48-7
• Molecular Formula: C₇H₈O₂S
• Molecular Weight: 160.207
• Mol file: 454705-48-7.mol

Synonyms:di-18(O)-methyl phenyl sulfone

Chemical Property of di-18(O)-methyl phenyl sulfone

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of di-18(O)-methyl phenyl sulfone

There total 3 articles about di-18(O)-methyl phenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

methyl-phenyl-thioether (100-68-5) → methyl phenyl [18O]sulfoxide (42463-36-5) + di-18(O)-methyl phenyl sulfone (454705-48-7)

Guidance literature:

With [(tris(6-methyl-2-pyridylmethyl)amine)Fe^II(benzilate)](ClO₄); oxygen-18; In acetonitrile; at 20 ℃; Reagent/catalyst;

DOI:10.1021/acs.inorgchem.6b02282

Reference yield:

methyl-phenyl-thioether (100-68-5) → methylphenylsulfonate (3112-85-4) + di-18(O)-methyl phenyl sulfone (454705-48-7) + [(18)O]methylsulfonylbenzene (1402140-22-0)

Guidance literature:

With tetrabutylammonium tetrafluoroborate; ¹⁸O-labeled water; In methanol; at 25 ℃; for 10h; Overall yield = 71 percent; Electrochemical reaction;

DOI:10.1021/acs.joc.1c01657

Reference yield:

methyl-phenyl-thioether (100-68-5) → di-18(O)-methyl phenyl sulfone (454705-48-7)

Guidance literature:

With hydrogen ⁽¹⁸⁾O-peroxide; myoglobin H₆₄D mutant; protoheme IX; at 25 ℃; pH=7; aq. buffer;

DOI:10.1002/asia.201100107

upstream raw materials:

methyl-phenyl-thioether