Phosphoric acid dibenzyl ester (1R,2R)-1-(tert-butyl-diphenyl-silanyloxymethyl)-2-octanoylamino-2-phenyl-ethyl ester

Base Information

Chemical Name:Phosphoric acid dibenzyl ester (1R,2R)-1-(tert-butyl-diphenyl-silanyloxymethyl)-2-octanoylamino-2-phenyl-ethyl ester
CAS No.:526217-41-4
Molecular Formula:C₄₇H₅₈NO₆PSi
Molecular Weight:792.04
Hs Code.:

Synonyms:Phosphoric acid dibenzyl ester (1R,2R)-1-(tert-butyl-diphenyl-silanyloxymethyl)-2-octanoylamino-2-phenyl-ethyl ester

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Chemical Property of Phosphoric acid dibenzyl ester (1R,2R)-1-(tert-butyl-diphenyl-silanyloxymethyl)-2-octanoylamino-2-phenyl-ethyl ester

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Technology Process of Phosphoric acid dibenzyl ester (1R,2R)-1-(tert-butyl-diphenyl-silanyloxymethyl)-2-octanoylamino-2-phenyl-ethyl ester

There total 6 articles about Phosphoric acid dibenzyl ester (1R,2R)-1-(tert-butyl-diphenyl-silanyloxymethyl)-2-octanoylamino-2-phenyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Phosphorous acid dibenzyl ester (1R,2R)-1-(tert-butyl-diphenyl-silanyloxymethyl)-2-octanoylamino-2-phenyl-ethyl ester

: 526217-41-4
Phosphoric acid dibenzyl ester (1R,2R)-1-(tert-butyl-diphenyl-silanyloxymethyl)-2-octanoylamino-2-phenyl-ethyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/S0968-0896(02)00380-2

Reference yield:

: 104196-23-8
(2S,3S)-2,3-epoxy-3-phenyl-1-propanol

: 526217-41-4
Phosphoric acid dibenzyl ester (1R,2R)-1-(tert-butyl-diphenyl-silanyloxymethyl)-2-octanoylamino-2-phenyl-ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 59 percent / NaN₃; NH₄Cl / dioxane; H₂O / 48 h / 80 °C

2: 6 M HCl; H₂ / 10 percent Pd/C / ethanol / 14 h / 20 °C

3: 83 percent / NaHCO₃ / tetrahydrofuran; H₂O / 7 h / 0 °C

4: 2.3 g / imidazole / dimethylformamide / 18 h / 20 °C

5: tetrazole / acetonitrile / 3 h / 20 °C

6: m-CPBA / CH₂Cl₂ / 1 h / 0 °C

With 1H-imidazole; 1H-tetrazole; hydrogenchloride; sodium azide; hydrogen; sodium hydrogencarbonate; ammonium chloride; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0968-0896(02)00380-2

Reference yield:

: 121745-57-1
(2R,3R)-3-azido-3-phenyl-propane-1,2diol

: 526217-41-4
Phosphoric acid dibenzyl ester (1R,2R)-1-(tert-butyl-diphenyl-silanyloxymethyl)-2-octanoylamino-2-phenyl-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 6 M HCl; H₂ / 10 percent Pd/C / ethanol / 14 h / 20 °C

2: 83 percent / NaHCO₃ / tetrahydrofuran; H₂O / 7 h / 0 °C

3: 2.3 g / imidazole / dimethylformamide / 18 h / 20 °C

4: tetrazole / acetonitrile / 3 h / 20 °C

5: m-CPBA / CH₂Cl₂ / 1 h / 0 °C

With 1H-imidazole; 1H-tetrazole; hydrogenchloride; hydrogen; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0968-0896(02)00380-2