2,6,10-tribenzyloxy-3,7,11-tri(tert-butyloxycarbonylmethoxy)triphenylene

Base Information

Chemical Name:2,6,10-tribenzyloxy-3,7,11-tri(tert-butyloxycarbonylmethoxy)triphenylene
CAS No.:198556-15-9
Molecular Formula:C₅₇H₆₀O₁₂
Molecular Weight:937.096
Hs Code.:

Synonyms:2,6,10-tribenzyloxy-3,7,11-tri(tert-butyloxycarbonylmethoxy)triphenylene

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Chemical Property of 2,6,10-tribenzyloxy-3,7,11-tri(tert-butyloxycarbonylmethoxy)triphenylene

Chemical Property:

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Technology Process of 2,6,10-tribenzyloxy-3,7,11-tri(tert-butyloxycarbonylmethoxy)triphenylene

There total 3 articles about 2,6,10-tribenzyloxy-3,7,11-tri(tert-butyloxycarbonylmethoxy)triphenylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 198556-13-7
2,6,10-tribenzyloxy-3,7,11-trihydroxytriphenylene

: 198556-15-9
2,6,10-tribenzyloxy-3,7,11-tri(tert-butyloxycarbonylmethoxy)triphenylene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 19h; Ambient temperature;
DOI:10.1055/s-1997-1309

Reference yield:

: 100-39-0
benzyl bromide

: 198556-15-9
2,6,10-tribenzyloxy-3,7,11-tri(tert-butyloxycarbonylmethoxy)triphenylene

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / K₂CO₃ / dimethylformamide / 18 h / Ambient temperature

2: 49 percent / 9-bromo-9-borabicyclo<3.3.1>nonane / CH₂Cl₂ / 0.67 h / -78 °C

3: 80 percent / K₂CO₃ / dimethylformamide / 19 h / Ambient temperature

With B-Br-9-BBN; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-1997-1309

Reference yield:

: 134025-09-5
2,3,6,7,10,11-hexabenzyloxytriphenylene

: 198556-15-9
2,6,10-tribenzyloxy-3,7,11-tri(tert-butyloxycarbonylmethoxy)triphenylene

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / 9-bromo-9-borabicyclo<3.3.1>nonane / CH₂Cl₂ / 0.67 h / -78 °C

2: 80 percent / K₂CO₃ / dimethylformamide / 19 h / Ambient temperature

With B-Br-9-BBN; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-1997-1309