3-(N-nonyl-N-benzoylamino)-5-(2'-(5',2'',5'',2'''-terthienyl))-N'-methylbenzanilide

Base Information

Chemical Name:3-(N-nonyl-N-benzoylamino)-5-(2'-(5',2'',5'',2'''-terthienyl))-N'-methylbenzanilide
CAS No.:1268704-13-7
Molecular Formula:C₄₂H₄₂N₂O₂S₃
Molecular Weight:703.006
Hs Code.:

Synonyms:3-(N-nonyl-N-benzoylamino)-5-(2'-(5',2'',5'',2'''-terthienyl))-N'-methylbenzanilide

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Chemical Property of 3-(N-nonyl-N-benzoylamino)-5-(2'-(5',2'',5'',2'''-terthienyl))-N'-methylbenzanilide

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Technology Process of 3-(N-nonyl-N-benzoylamino)-5-(2'-(5',2'',5'',2'''-terthienyl))-N'-methylbenzanilide

There total 6 articles about 3-(N-nonyl-N-benzoylamino)-5-(2'-(5',2'',5'',2'''-terthienyl))-N'-methylbenzanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1268704-11-5
3-(N-nonyl-N-benzoylamino)-5-bromo-N'-methylbenzanilide

: 205235-02-5
(2,2’:5’,2’’-terthiophen)-5-ylboronic acid

: 1268704-13-7
3-(N-nonyl-N-benzoylamino)-5-(2'-(5',2'',5'',2'''-terthienyl))-N'-methylbenzanilide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; Reflux;
DOI:10.1021/jo102160x

Reference yield:

: 6307-83-1
3-bromo-5-nitro-benzoic acid

: 1268704-13-7
3-(N-nonyl-N-benzoylamino)-5-(2'-(5',2'',5'',2'''-terthienyl))-N'-methylbenzanilide

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride / 6 h / 0 °C / Reflux

2: tin(ll) chloride / tetrahydrofuran; ethanol / 6 h / 0 °C / Reflux

3: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran / 20 °C

4: pyridine / 2 h / 80 °C

5: lithium hexamethyldisilazane / 2 h / 0 °C

6: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; tin(ll) chloride; lithium hexamethyldisilazane; In tetrahydrofuran; pyridine; ethanol; water;
DOI:10.1021/jo102160x

Reference yield:

: methyl 3-(N-nonyl-N-benzoylamino)-5-bromobenzoate

: 1268704-13-7
3-(N-nonyl-N-benzoylamino)-5-(2'-(5',2'',5'',2'''-terthienyl))-N'-methylbenzanilide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hexamethyldisilazane / 2 h / 0 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; water;
DOI:10.1021/jo102160x