1(E)-hexa-1,4-dienylbenzene

Base Information

Chemical Name:1(E)-hexa-1,4-dienylbenzene
CAS No.:163976-68-9
Molecular Formula:C₁₂H₁₄
Molecular Weight:158.243
Hs Code.:

Synonyms:1(E)-hexa-1,4-dienylbenzene

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Chemical Property of 1(E)-hexa-1,4-dienylbenzene

Chemical Property:

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Technology Process of 1(E)-hexa-1,4-dienylbenzene

There total 5 articles about 1(E)-hexa-1,4-dienylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 124745-29-5,124745-65-9,124745-66-0
(E)-4-<(1-ethenyl-4-phenylbut-3-enyl)sulfinyl>morpholine

: 163976-68-9
1(E)-hexa-1,4-dienylbenzene

Guidance literature:: With water; In 1,4-dioxane; at 0 ℃; for 2h;

Reference yield:

: 124831-13-6
((E)-But-2-enyl)-methyl-diphenyl-phosphonium; iodide

: 100-52-7
benzaldehyde

: 163976-68-9
1(E)-hexa-1,4-dienylbenzene

: 2129-89-7
diphenyl(methyl)phosphine oxide

Guidance literature:: With potassium carbonate; In methanol;

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 56644-04-3
(E)-1-phenyl-1,5-hexadiene

: 163976-68-9
1(E)-hexa-1,4-dienylbenzene

: 109898-18-2
(E)-(4-methylpenta-1,4-dien-1-yl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 15 h / 0 °C / Reflux; Inert atmosphere

2: bis(1,5-cyclooctadiene)nickel⁽⁰⁾; tris(o-methoxyphenyl)phosphine; triethylsilyl trifluoromethyl sulfonate; triethylamine / toluene / 3.5 h / 20 °C / 760.05 Torr / Inert atmosphere

With pyridine; bis(1,5-cyclooctadiene)nickel⁽⁰⁾; tris(o-methoxyphenyl)phosphine; triethylsilyl trifluoromethyl sulfonate; triethylamine; In dichloromethane; toluene;
DOI:10.1002/asia.201000875