4-Chloro-1-<2-deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl>-1H-imidazo<4,5-c>pyridine

Base Information

Chemical Name:4-Chloro-1-<2-deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl>-1H-imidazo<4,5-c>pyridine
CAS No.:78582-13-5
Molecular Formula:C₂₇H₂₄ClN₃O₅
Molecular Weight:505.958
Hs Code.:

Synonyms:4-Chloro-1-<2-deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl>-1H-imidazo<4,5-c>pyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Chloro-1-<2-deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl>-1H-imidazo<4,5-c>pyridine

Chemical Property:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 4-Chloro-1-<2-deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl>-1H-imidazo<4,5-c>pyridine

There total 1 articles about 4-Chloro-1-<2-deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl>-1H-imidazo<4,5-c>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 2770-01-6
4-chloro-1H-imidazo[4,5-c]pyridine

: 4330-21-6
2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

: 130948-29-7
4-Chloro-3-<2-deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl>-1H-imidazo<4,5-c>pyridine

: 78582-13-5
4-Chloro-1-<2-deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl>-1H-imidazo<4,5-c>pyridine

Guidance literature:: With potassium hydroxide; Tris(3,6-dioxaheptyl)amine; In acetonitrile; for 1h; Ambient temperature;

Reference yield: 92.0%

: 78582-13-5
4-Chloro-1-<2-deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl>-1H-imidazo<4,5-c>pyridine

: 78582-15-7
4-chloro-1-(2'-deoxy-β-D-erythro-pentofuranosyl)-1H-imidazo<4,5-c>pyridine

Guidance literature:: With ammonia; for 16h; Ambient temperature;

Reference yield:

: 78582-13-5
4-Chloro-1-<2-deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl>-1H-imidazo<4,5-c>pyridine

: 130948-32-2
4-Chloro-1-<2,3-dideoxy-5-O-(4-methoxytrityl)-β-D-glyceropentofuranosyl>-1H-imidazo<4,5-c>pyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / methanolic NH₃ / 16 h / Ambient temperature

2: 82 percent / AgNO₃, pyridine / tetrahydrofuran / 3.5 h / Ambient temperature

3: 85 percent / DMAP / acetonitrile / 28 h / Ambient temperature

4: 90 percent / Bu₃SnH, 2,2'-azobis(2-methylpropionitrile) / benzene / 0.33 h / Heating

With pyridine; dmap; 2,2'-azobis(isobutyronitrile); ammonia; tri-n-butyl-tin hydride; silver nitrate; In tetrahydrofuran; acetonitrile; benzene;