2-{3-phenyl-1-[2-(4-chlorophenyl)ethenyl]-2-propen-1-ylidene}-hydrazinecarboximidamide hydrochloride

Base Information

Chemical Name:2-{3-phenyl-1-[2-(4-chlorophenyl)ethenyl]-2-propen-1-ylidene}-hydrazinecarboximidamide hydrochloride
CAS No.:1384457-86-6
Molecular Formula:C₁₈H₁₇ClN₄*ClH
Molecular Weight:361.274
Hs Code.:

Synonyms:2-{3-phenyl-1-[2-(4-chlorophenyl)ethenyl]-2-propen-1-ylidene}-hydrazinecarboximidamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-{3-phenyl-1-[2-(4-chlorophenyl)ethenyl]-2-propen-1-ylidene}-hydrazinecarboximidamide hydrochloride

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Technology Process of 2-{3-phenyl-1-[2-(4-chlorophenyl)ethenyl]-2-propen-1-ylidene}-hydrazinecarboximidamide hydrochloride

There total 2 articles about 2-{3-phenyl-1-[2-(4-chlorophenyl)ethenyl]-2-propen-1-ylidene}-hydrazinecarboximidamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 68386-89-0,79462-12-7,79462-15-0,34292-83-6
1-(4-chlorophenyl)-5-phenyl-penta-1,4-dien-3-one

: 1937-19-5,16139-18-7
1-aminoguanidine hydrochloride

: 1384457-86-6
2-{3-phenyl-1-[2-(4-chlorophenyl)ethenyl]-2-propen-1-ylidene}-hydrazinecarboximidamide hydrochloride

Guidance literature:: With para-dodecylbenzenesulfonic acid; In water; at 25 - 27 ℃; for 2.5h; Sonication;
DOI:10.1016/j.ultsonch.2012.02.009

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 100-52-7
benzaldehyde

: 1384457-86-6
2-{3-phenyl-1-[2-(4-chlorophenyl)ethenyl]-2-propen-1-ylidene}-hydrazinecarboximidamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol; water / Sonication

2: para-dodecylbenzenesulfonic acid / water / 2.5 h / 25 - 27 °C / Sonication

With para-dodecylbenzenesulfonic acid; potassium hydroxide; In ethanol; water;
DOI:10.1016/j.ultsonch.2012.02.009