Isobutyric acid (3S,6S,7R,8R)-8-(4-amino-benzyl)-3-[(3-hydroxy-4-methoxy-pyridine-2-carbonyl)-amino]-6-methyl-4,9-dioxo-[1,5]dioxonan-7-yl ester

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Chemical Name:Isobutyric acid (3S,6S,7R,8R)-8-(4-amino-benzyl)-3-[(3-hydroxy-4-methoxy-pyridine-2-carbonyl)-amino]-6-methyl-4,9-dioxo-[1,5]dioxonan-7-yl ester
CAS No.:234113-27-0
Molecular Formula:C₂₆H₃₁N₃O₉
Molecular Weight:529.547
Hs Code.:
Mol file:234113-27-0.mol

Synonyms:Isobutyric acid (3S,6S,7R,8R)-8-(4-amino-benzyl)-3-[(3-hydroxy-4-methoxy-pyridine-2-carbonyl)-amino]-6-methyl-4,9-dioxo-[1,5]dioxonan-7-yl ester

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Chemical Property of Isobutyric acid (3S,6S,7R,8R)-8-(4-amino-benzyl)-3-[(3-hydroxy-4-methoxy-pyridine-2-carbonyl)-amino]-6-methyl-4,9-dioxo-[1,5]dioxonan-7-yl ester Edit

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Technology Process of Isobutyric acid (3S,6S,7R,8R)-8-(4-amino-benzyl)-3-[(3-hydroxy-4-methoxy-pyridine-2-carbonyl)-amino]-6-methyl-4,9-dioxo-[1,5]dioxonan-7-yl ester

There total 2 articles about Isobutyric acid (3S,6S,7R,8R)-8-(4-amino-benzyl)-3-[(3-hydroxy-4-methoxy-pyridine-2-carbonyl)-amino]-6-methyl-4,9-dioxo-[1,5]dioxonan-7-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 234113-26-9
Isobutyric acid (3S,6S,7R,8R)-3-[(3-hydroxy-4-methoxy-pyridine-2-carbonyl)-amino]-6-methyl-8-(4-nitro-benzyl)-4,9-dioxo-[1,5]dioxonan-7-yl ester

: 234113-27-0
Isobutyric acid (3S,6S,7R,8R)-8-(4-amino-benzyl)-3-[(3-hydroxy-4-methoxy-pyridine-2-carbonyl)-amino]-6-methyl-4,9-dioxo-[1,5]dioxonan-7-yl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1016/j.bmcl.2005.02.065

Reference yield:

: 167173-85-5
(3S,6S,7R,8R)-8-benzyl-3-{[(3-hydroxy-4-methoxypyridin-2-yl)carbonyl]amino}-6-methyl-4,9-dioxo-1,5-dioxonan-7-yl2-methylpropanoate

: 234113-27-0
Isobutyric acid (3S,6S,7R,8R)-8-(4-amino-benzyl)-3-[(3-hydroxy-4-methoxy-pyridine-2-carbonyl)-amino]-6-methyl-4,9-dioxo-[1,5]dioxonan-7-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / HNO₃ / CH₂Cl₂ / -20 °C

2: 72 percent / H₂ / Pd/C / ethanol

With hydrogen; nitric acid; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2005.02.065