(R)-tert-butyl(1-(furan-2-yl)tridecyloxy)diphenylsilane

Base Information

Chemical Name:(R)-tert-butyl(1-(furan-2-yl)tridecyloxy)diphenylsilane
CAS No.:1344148-78-2
Molecular Formula:C₃₃H₄₈O₂Si
Molecular Weight:504.828
Hs Code.:

Synonyms:(R)-tert-butyl(1-(furan-2-yl)tridecyloxy)diphenylsilane

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Chemical Property of (R)-tert-butyl(1-(furan-2-yl)tridecyloxy)diphenylsilane

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Technology Process of (R)-tert-butyl(1-(furan-2-yl)tridecyloxy)diphenylsilane

There total 11 articles about (R)-tert-butyl(1-(furan-2-yl)tridecyloxy)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353388-71-2
C₃₇H₆₀O₄Si

: 1344148-78-2
(R)-tert-butyl(1-(furan-2-yl)tridecyloxy)diphenylsilane

Guidance literature:: With hydrogenchloride; water; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetlet.2011.08.160

Reference yield:

: 1344148-85-1
(R)-methyl 4-(tert-butyldimethylsilyloxy)-2-(tert-butyldiphenylsilyloxy)butanoate

: 1344148-78-2
(R)-tert-butyl(1-(furan-2-yl)tridecyloxy)diphenylsilane

Guidance literature:: Multi-step reaction with 11 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 7 h / -78 °C

2.1: pyridine; dmap / 3 h / 0 - 20 °C

3.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 7 h / 0 - 20 °C

4.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 6 h / 20 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C

5.2: 0.17 h / 0 °C

6.1: palladium 10% on activated carbon; hydrogen / methanol / 41 h / 20 °C

7.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

8.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 8 h / 20 °C

9.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - 0 °C

9.2: 0.67 h / -78 - 20 °C

10.1: hydrogen / hexane / 0.92 h / 20 °C

11.1: hydrogenchloride; water / dichloromethane / 20 °C

With pyridine; hydrogenchloride; dmap; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; pyridine hydrofluoride; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; water; hydrogen; diisobutylaluminium hydride; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene; 5.1: Wittig reaction / 5.2: Wittig reaction;
DOI:10.1016/j.tetlet.2011.08.160

Reference yield:

: 1344148-86-2
(R)-4-(tert-butyldimethylsilyloxy)-2-(tert-butyldiphenylsilyloxy)butan-1-ol

: 1344148-78-2
(R)-tert-butyl(1-(furan-2-yl)tridecyloxy)diphenylsilane

Guidance literature:: Multi-step reaction with 10 steps

1.1: pyridine; dmap / 3 h / 0 - 20 °C

2.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 7 h / 0 - 20 °C

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 6 h / 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C

4.2: 0.17 h / 0 °C

5.1: palladium 10% on activated carbon; hydrogen / methanol / 41 h / 20 °C

6.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

7.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 8 h / 20 °C

8.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - 0 °C

8.2: 0.67 h / -78 - 20 °C

9.1: hydrogen / hexane / 0.92 h / 20 °C

10.1: hydrogenchloride; water / dichloromethane / 20 °C

With pyridine; hydrogenchloride; dmap; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; pyridine hydrofluoride; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; water; hydrogen; diisobutylaluminium hydride; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene; 4.1: Wittig reaction / 4.2: Wittig reaction;
DOI:10.1016/j.tetlet.2011.08.160