O-benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(2,2-dimethyl-1,3-dioxan-5-yl)phenol

Base Information

Chemical Name:O-benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(2,2-dimethyl-1,3-dioxan-5-yl)phenol
CAS No.:144667-28-7
Molecular Formula:C₃₃H₃₂N₂O₅
Molecular Weight:536.627
Hs Code.:

O-benzyl-N<sup>2</sup>,N<sup>5</sup>-dibenzoyl-2,5-diamino-4-(2,2-dimethyl-1,3-dioxan-5-yl)phenol

Synonyms:O-benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(2,2-dimethyl-1,3-dioxan-5-yl)phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(2,2-dimethyl-1,3-dioxan-5-yl)phenol

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Technology Process of O-benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(2,2-dimethyl-1,3-dioxan-5-yl)phenol

There total 4 articles about O-benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(2,2-dimethyl-1,3-dioxan-5-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 144667-27-6
O-benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(bis(hydroxymethyl)methyl)phenol

: 77-76-9
2,2-dimethoxy-propane

: 144667-28-7
O-benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(2,2-dimethyl-1,3-dioxan-5-yl)phenol

Guidance literature:: With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 25 ℃; for 24h;
DOI:10.1021/ja00073a019

Reference yield:

: 124400-60-8
O-Benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(1,1-bis(methoxycarbonyl)methyl)phenol

: 144667-28-7
O-benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(2,2-dimethyl-1,3-dioxan-5-yl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / NaBH₄ / ethanol / a) 0 deg C, 30 min, b) 25 deg C, 2.5 h

2: 100 percent / TsOH / dimethylformamide / 24 h / 25 °C

With sodium tetrahydroborate; toluene-4-sulfonic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja00073a019

Reference yield:

: C₂₇H₂₀N₂O₃

: 144667-28-7
O-benzyl-N²,N⁵-dibenzoyl-2,5-diamino-4-(2,2-dimethyl-1,3-dioxan-5-yl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1: NaOCH₃ / tetrahydrofuran / 2 h / -30 °C

2: 71 percent / NaBH₄ / ethanol / a) 0 deg C, 30 min, b) 25 deg C, 2.5 h

3: 100 percent / TsOH / dimethylformamide / 24 h / 25 °C

With sodium tetrahydroborate; sodium methylate; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja00073a019