lithium salt of 4-(5-chloro-6-methoxypyridin-3-yloxy)-2,5-difluorobenzoic acid

Base Information

Chemical Name:lithium salt of 4-(5-chloro-6-methoxypyridin-3-yloxy)-2,5-difluorobenzoic acid
CAS No.:1355066-43-1
Molecular Formula:C₁₃H₇ClF₂NO₄*Li
Molecular Weight:321.594
Hs Code.:

Synonyms:lithium salt of 4-(5-chloro-6-methoxypyridin-3-yloxy)-2,5-difluorobenzoic acid

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Chemical Property of lithium salt of 4-(5-chloro-6-methoxypyridin-3-yloxy)-2,5-difluorobenzoic acid

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Technology Process of lithium salt of 4-(5-chloro-6-methoxypyridin-3-yloxy)-2,5-difluorobenzoic acid

There total 3 articles about lithium salt of 4-(5-chloro-6-methoxypyridin-3-yloxy)-2,5-difluorobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1355066-44-2
tert-butyl 4-(5-chloro-6-methoxypyridin-3-yloxy)-2,5-difluorobenzoate

: 1355066-43-1
lithium salt of 4-(5-chloro-6-methoxypyridin-3-yloxy)-2,5-difluorobenzoic acid

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

Reference yield:

: 446-17-3
2,4,5-trifluorobenzoic acid

: 1355066-43-1
lithium salt of 4-(5-chloro-6-methoxypyridin-3-yloxy)-2,5-difluorobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / tert-butyl alcohol / 16 h / 30 °C / Inert atmosphere

2: potassium carbonate / dimethyl sulfoxide / 25 °C / Inert atmosphere

3: water; lithium hydroxide / tetrahydrofuran / 20 °C / Inert atmosphere

With water; potassium carbonate; lithium hydroxide; dmap; In tetrahydrofuran; dimethyl sulfoxide; tert-butyl alcohol;

Reference yield:

: 182875-05-4
tert-butyl 2,4,5-trifluorobenzoate

: 1355066-43-1
lithium salt of 4-(5-chloro-6-methoxypyridin-3-yloxy)-2,5-difluorobenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dimethyl sulfoxide / 25 °C / Inert atmosphere

2: water; lithium hydroxide / tetrahydrofuran / 20 °C / Inert atmosphere

With water; potassium carbonate; lithium hydroxide; In tetrahydrofuran; dimethyl sulfoxide;