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C34H59N3O14

Base Information
  • Chemical Name:C34H59N3O14
  • CAS No.:1374760-32-3
  • Molecular Formula:C34H59N3O14
  • Molecular Weight:733.854
  • Hs Code.:
C<sub>34</sub>H<sub>59</sub>N<sub>3</sub>O<sub>14</sub>

Synonyms:C34H59N3O14

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Chemical Property of C34H59N3O14
Chemical Property:
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98% *data from raw suppliers

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Technology Process of C34H59N3O14

There total 22 articles about C34H59N3O14 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
at 80 ℃; for 8h;
Guidance literature:
Multi-step reaction with 7 steps
1.1: sodium methylate; methanol / 2 h
1.2: IR-120 (H(1+)) resin
2.1: triethylamine / acetonitrile / 1.33 h / 0 °C
3.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux
3.2: 20 °C
4.1: tri-n-butyl-tin hydride / Pd(Ph)4 / dichloromethane / 1 h / 20 °C
5.1: hydrogen; acetic acid / palladium 10% on activated carbon / 1,4-dioxane; water / 5 h / 20 °C / 1034.32 Torr
6.1: sodium methylate; methanol / 4 h
6.2: IR-120 (H(1+)) resin
7.1: 8 h / 80 °C
With methanol; hydrogen; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; acetic acid; triethylamine; palladium 10% on activated carbon; In 1,4-dioxane; methanol; dichloromethane; water; acetonitrile;
Guidance literature:
Multi-step reaction with 10 steps
1.1: ammonium acetate / N,N-dimethyl-formamide / 20 - 50 °C / Inert atmosphere
2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.5 h / 20 °C
3.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve
3.2: 2 h / 0 °C
4.1: sodium methylate; methanol / 2 h
4.2: IR-120 (H(1+)) resin
5.1: triethylamine / acetonitrile / 1.33 h / 0 °C
6.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux
6.2: 20 °C
7.1: tri-n-butyl-tin hydride / Pd(Ph)4 / dichloromethane / 1 h / 20 °C
8.1: hydrogen; acetic acid / palladium 10% on activated carbon / 1,4-dioxane; water / 5 h / 20 °C / 1034.32 Torr
9.1: sodium methylate; methanol / 4 h
9.2: IR-120 (H(1+)) resin
10.1: 8 h / 80 °C
With methanol; ammonium acetate; hydrogen; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; palladium 10% on activated carbon; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
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