4-bromo-benzenesulfonic acid methallylamide

Base Information

• Chemical Name: 4-bromo-benzenesulfonic acid methallylamide
• CAS No.: 1206-40-2
• Molecular Formula: C₁₀H₁₂BrNO₂S
• Molecular Weight: 290.181
• Mol file: 1206-40-2.mol

Synonyms:4-bromo-benzenesulfonic acid methallylamide

Chemical Property of 4-bromo-benzenesulfonic acid methallylamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 4-bromo-benzenesulfonic acid methallylamide

There total 2 articles about 4-bromo-benzenesulfonic acid methallylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-bromobenzenesulfonyl chloride (98-58-8) + 2-methylallylamin (2878-14-0) → 4-bromo-benzenesulfonic acid methallylamide (1206-40-2)

Guidance literature:

DOI:10.1021/ja01878a059

Reference yield:

→ 4-bromo-benzenesulfonic acid methallylamide (1206-40-2)

Guidance literature:

4-Brom-phenylsulfonamid, 2-Methyl-allylchlorid, wss.-ethanol. NaOH, Erwaermen;

Reference yield: 50.0%

(3-(cyclohexylidenemethylene)-2,2-dimethylcyclopropyl)methanol (38387-24-5) + 4-bromo-benzenesulfonic acid methallylamide (1206-40-2) → 4-bromo-N-((3-(cyclohexylidenemethylene)-2,2-dimethylcyclopropyl)methyl)-N-(2-methylallyl)benzenesulfonamide (1381807-98-2)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/om3004288

upstream raw materials:

4-bromobenzenesulfonyl chloride

2-methylallylamin

Downstream raw materials:

C₂₀H₂₆BrNO₂S

4-bromo-N-((3-(cyclohexylidenemethylene)-2,2-dimethylcyclopropyl)methyl)-N-(2-methylallyl)benzenesulfonamide