diethyl (1S,2R)-1-(3,4,5-trimethoxyphenyl)-6,7,8-trimethoxy-1,2-dihydronaphthalene-2,3-dicarboxylate

Base Information

Chemical Name:diethyl (1S,2R)-1-(3,4,5-trimethoxyphenyl)-6,7,8-trimethoxy-1,2-dihydronaphthalene-2,3-dicarboxylate
CAS No.:721396-17-4
Molecular Formula:C₂₈H₃₄O₁₀
Molecular Weight:530.572
Hs Code.:

Synonyms:diethyl (1S,2R)-1-(3,4,5-trimethoxyphenyl)-6,7,8-trimethoxy-1,2-dihydronaphthalene-2,3-dicarboxylate

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Chemical Property of diethyl (1S,2R)-1-(3,4,5-trimethoxyphenyl)-6,7,8-trimethoxy-1,2-dihydronaphthalene-2,3-dicarboxylate

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Technology Process of diethyl (1S,2R)-1-(3,4,5-trimethoxyphenyl)-6,7,8-trimethoxy-1,2-dihydronaphthalene-2,3-dicarboxylate

There total 1 articles about diethyl (1S,2R)-1-(3,4,5-trimethoxyphenyl)-6,7,8-trimethoxy-1,2-dihydronaphthalene-2,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-17-5
ethanol

: (1S,2R)-1-(3,4,5-trimethoxyphenyl)-6,7,8-trimethoxy-1,2-dihydronaphthalene-2,3-dicarboxylic acid

: 721396-17-4
diethyl (1S,2R)-1-(3,4,5-trimethoxyphenyl)-6,7,8-trimethoxy-1,2-dihydronaphthalene-2,3-dicarboxylate

Guidance literature:: With sulfuric acid; Heating;
DOI:10.1021/jo0497454

Reference yield:

: 721396-17-4
diethyl (1S,2R)-1-(3,4,5-trimethoxyphenyl)-6,7,8-trimethoxy-1,2-dihydronaphthalene-2,3-dicarboxylate

: diethyl (1S,2R)-1-(3,4,5-trimethoxyphenyl)-6,7,8-trimethoxy-1,2,3,4-tetrahydronaphthalene-2,3-dicarboxylate

: diethyl (1S,2R)-1-(3,4,5-trimethoxyphenyl)-6,7,8-trimethoxy-1,2,3,4-tetrahydronaphthalene-2,3-dicarboxylate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; Title compound not separated from byproducts;
DOI:10.1021/jo0497454

Reference yield:

: 721396-17-4
diethyl (1S,2R)-1-(3,4,5-trimethoxyphenyl)-6,7,8-trimethoxy-1,2-dihydronaphthalene-2,3-dicarboxylate

: 54712-60-6
lyoniresinol dimethyl ether

: 73745-48-9
epilyoniresinol dimethyl ether

Guidance literature:: diethyl (1S,2R)-1-(3,4,5-trimethoxyphenyl)-6,7,8-trimethoxy-1,2-dihydronaphthalene-2,3-dicarboxylate; With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃;

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1021/jo0497454