(Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenylsulfanyl]-phenyl}-propenal

Base Information

Chemical Name:(Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenylsulfanyl]-phenyl}-propenal
CAS No.:1021942-60-8
Molecular Formula:C₁₈H₁₂Cl₂O₂S
Molecular Weight:363.264
Hs Code.:

Synonyms:(Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenylsulfanyl]-phenyl}-propenal

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Chemical Property of (Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenylsulfanyl]-phenyl}-propenal

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Technology Process of (Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenylsulfanyl]-phenyl}-propenal

There total 2 articles about (Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenylsulfanyl]-phenyl}-propenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 2615-09-0
bis(4-acetylphenyl)sulfide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1021942-60-8
(Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenylsulfanyl]-phenyl}-propenal

Guidance literature:: N,N-dimethyl-formamide; With trichlorophosphate; at 0 ℃; for 0.166667h;

bis(4-acetylphenyl)sulfide; In N,N-dimethyl-formamide; at 4 ℃; for 120h;
DOI:10.1016/S0040-4020(01)00676-7

Reference yield:

: 139-66-2
diphenyl sulfide

: 1021942-60-8
(Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenylsulfanyl]-phenyl}-propenal

Guidance literature:: Multi-step reaction with 2 steps

1.1: 71 percent / AlCl₃ / CS₂

2.1: POCl₃ / 0.17 h / 0 °C

2.2: 78 percent / dimethylformamide / 120 h / 4 °C

With aluminium trichloride; trichlorophosphate; In carbon disulfide; 1.1: Friedel-Crafts acylation;
DOI:10.1016/S0040-4020(01)00676-7

Reference yield: 78.0%

: 2365-48-2
Methyl thioglycolate

: 1021942-60-8
(Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenylsulfanyl]-phenyl}-propenal

: 361391-40-4
C₂₄H₁₈O₄S₃

Guidance literature:: Methyl thioglycolate; (Z)-3-Chloro-3-{4-[4-((Z)-1-chloro-3-oxo-propenyl)-phenylsulfanyl]-phenyl}-propenal; With triethylamine; In pyridine; at 0 - 50 ℃;

With potassium hydroxide; In pyridine; water; at 10 - 15 ℃; for 0.333333h;
DOI:10.1016/S0040-4020(01)00676-7