1-phthalimido-4-[(N-phenylsulfonyl)-3-indolyl]-2-triisopropylsiloxy-1,3-butadiene

Base Information

Chemical Name:1-phthalimido-4-[(N-phenylsulfonyl)-3-indolyl]-2-triisopropylsiloxy-1,3-butadiene
CAS No.:679005-02-8
Molecular Formula:C₃₅H₃₈N₂O₅SSi
Molecular Weight:626.849
Hs Code.:

Synonyms:1-phthalimido-4-[(N-phenylsulfonyl)-3-indolyl]-2-triisopropylsiloxy-1,3-butadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phthalimido-4-[(N-phenylsulfonyl)-3-indolyl]-2-triisopropylsiloxy-1,3-butadiene

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Technology Process of 1-phthalimido-4-[(N-phenylsulfonyl)-3-indolyl]-2-triisopropylsiloxy-1,3-butadiene

There total 3 articles about 1-phthalimido-4-[(N-phenylsulfonyl)-3-indolyl]-2-triisopropylsiloxy-1,3-butadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 679005-01-7
2-[4-(1-benzenesulfonyl-1H-indol-3-yl)-2-oxo-but-3-enyl]-isoindole-1,3-dione

: 679005-02-8
1-phthalimido-4-[(N-phenylsulfonyl)-3-indolyl]-2-triisopropylsiloxy-1,3-butadiene

Guidance literature:: With triethylamine; In dichloromethane; at 50 ℃; for 2h;
DOI:10.1016/j.tetlet.2003.12.118

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 679005-01-7
2-[4-(1-benzenesulfonyl-1H-indol-3-yl)-2-oxo-but-3-enyl]-isoindole-1,3-dione

: 679005-02-8
1-phthalimido-4-[(N-phenylsulfonyl)-3-indolyl]-2-triisopropylsiloxy-1,3-butadiene

: 2-[(1E,3E)-4-(1-Benzenesulfonyl-1H-indol-3-yl)-2-triisopropylsilanyloxy-buta-1,3-dienyl]-isoindole-1,3-dione

Guidance literature:: With triethylamine; In dichloromethane; at 50 ℃; for 3h;
DOI:10.1016/j.tet.2005.04.076

Reference yield:

: 96056-26-7
2-[2-oxo-3-(triphenyl-λ⁵-phosphanylidene)propyl]-1H-isoindole-1,3(2H)-dione

: 679005-02-8
1-phthalimido-4-[(N-phenylsulfonyl)-3-indolyl]-2-triisopropylsiloxy-1,3-butadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / benzene / 2 h / Heating

2: Et₃N / CH₂Cl₂ / 2 h / 50 °C

With triethylamine; In dichloromethane; benzene;
DOI:10.1016/j.tet.2005.04.076