(1S,2S,5R)-2-isopropyl-5-methylcyclohexyl 4-(pentatriacontan-18-ylsulfonyl)benzoate

Base Information

Chemical Name:(1S,2S,5R)-2-isopropyl-5-methylcyclohexyl 4-(pentatriacontan-18-ylsulfonyl)benzoate
CAS No.:1399816-52-4
Molecular Formula:C₅₂H₉₄O₄S
Molecular Weight:815.382
Hs Code.:

Synonyms:(1S,2S,5R)-2-isopropyl-5-methylcyclohexyl 4-(pentatriacontan-18-ylsulfonyl)benzoate

Suppliers and Price of (1S,2S,5R)-2-isopropyl-5-methylcyclohexyl 4-(pentatriacontan-18-ylsulfonyl)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (1S,2S,5R)-2-isopropyl-5-methylcyclohexyl 4-(pentatriacontan-18-ylsulfonyl)benzoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (1S,2S,5R)-2-isopropyl-5-methylcyclohexyl 4-(pentatriacontan-18-ylsulfonyl)benzoate

There total 3 articles about (1S,2S,5R)-2-isopropyl-5-methylcyclohexyl 4-(pentatriacontan-18-ylsulfonyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2216-51-5
(-)-menthol

: 1399816-69-3
4-(pentatriacontan-18-ylsulfonyl)benzoic acid

: 1399816-52-4
(1S,2S,5R)-2-isopropyl-5-methylcyclohexyl 4-(pentatriacontan-18-ylsulfonyl)benzoate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1055/s-0031-1290406

Reference yield:

: 1399816-67-1
methyl 4-(pentatriacontan-18-ylsulfonyl)benzoate

: 1399816-52-4
(1S,2S,5R)-2-isopropyl-5-methylcyclohexyl 4-(pentatriacontan-18-ylsulfonyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 0 °C / Inert atmosphere

1.2: pH < 2 / Inert atmosphere

2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; water; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 2.1: Mitsunobu reaction;
DOI:10.1055/s-0031-1290406

Reference yield:

: 504-53-0
di-n-heptadecyl ketone

: 1399816-52-4
(1S,2S,5R)-2-isopropyl-5-methylcyclohexyl 4-(pentatriacontan-18-ylsulfonyl)benzoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 40 °C / Inert atmosphere

2.1: triethylamine / tetrahydrofuran; dichloromethane / 2 h / 20 - 35 °C / Inert atmosphere

3.1: caesium carbonate / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.08 h / 20 °C / Inert atmosphere

5.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 0 °C / Inert atmosphere

5.2: pH < 2 / Inert atmosphere

6.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; lithium hydroxide monohydrate; water; caesium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 6.1: Mitsunobu reaction;
DOI:10.1055/s-0031-1290406