C₂₄H₂₁N₅O₃

Base Information

Chemical Name:C₂₄H₂₁N₅O₃
CAS No.:1251589-03-3
Molecular Formula:C₂₄H₂₁N₅O₃
Molecular Weight:427.462
Hs Code.:

C<sub>24</sub>H<sub>21</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₂₄H₂₁N₅O₃

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Chemical Property of C₂₄H₂₁N₅O₃

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Technology Process of C₂₄H₂₁N₅O₃

There total 8 articles about C₂₄H₂₁N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 557-21-1
zinc(II) cyanide

: 1251582-27-0
C₂₃H₂₁BrN₄O₃

: 1251589-03-3
C₂₄H₂₁N₅O₃

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ISOPROPYLAMIDE; at 125 ℃; for 0.75h; Inert atmosphere; Microwave irradiation;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1251589-03-3
C₂₄H₂₁N₅O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium carbonate / acetone / 16 h / 75 °C

1.2: 0.25 h / 65 °C

2.1: potassium carbonate / toluene / 16 h / Reflux

3.1: sodium hydride / N,N-dimethyl-formamide / 0.75 h / 20 °C

3.2: 2 h / 20 - 90 °C

4.1: ammonium acetate / 2 h / 140 °C

4.2: pH 8 / Heating

5.1: triethylamine / dichloromethane / 1 h / 20 °C

6.1: triethylamine; sodium iodide / N,N-dimethyl-formamide / 70 °C

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ISOPROPYLAMIDE / 0.75 h / 125 °C / Inert atmosphere; Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium acetate; sodium hydride; sodium carbonate; potassium carbonate; triethylamine; sodium iodide; In dichloromethane; ISOPROPYLAMIDE; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: C₁₅H₁₀BrNO₂

: 1251589-03-3
C₂₄H₂₁N₅O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / toluene / 16 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.75 h / 20 °C

2.2: 2 h / 20 - 90 °C

3.1: ammonium acetate / 2 h / 140 °C

3.2: pH 8 / Heating

4.1: triethylamine / dichloromethane / 1 h / 20 °C

5.1: triethylamine; sodium iodide / N,N-dimethyl-formamide / 70 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ISOPROPYLAMIDE / 0.75 h / 125 °C / Inert atmosphere; Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium acetate; sodium hydride; potassium carbonate; triethylamine; sodium iodide; In dichloromethane; ISOPROPYLAMIDE; N,N-dimethyl-formamide; toluene;