4'-amino-3'-phenoxyacetophenone

Base Information

Chemical Name:4'-amino-3'-phenoxyacetophenone
CAS No.:116687-02-6
Molecular Formula:C₁₄H₁₃NO₂
Molecular Weight:227.263
Hs Code.:

Synonyms:4'-amino-3'-phenoxyacetophenone

Suppliers and Price of 4'-amino-3'-phenoxyacetophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 4'-amino-3'-phenoxyacetophenone

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4'-amino-3'-phenoxyacetophenone

There total 3 articles about 4'-amino-3'-phenoxyacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116687-01-5
4'-nitro-3'-phenoxyacetophenone

: 116687-02-6
4'-amino-3'-phenoxyacetophenone

Guidance literature:: With ammonium chloride; water; iron; In ethanol; for 0.5h; Heating;
DOI:10.1248/cpb.40.2399

Reference yield:

: 6953-83-9
1-(4-amino-3-chlorophenyl)ethan-1-one

: 116687-02-6
4'-amino-3'-phenoxyacetophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium nitrite, aq. HCl, 2.) sodium nitrite, cuprous oxide / 1.) from -5 deg C to 0 deg C, 10 min, 2.) H₂O, from -5 deg C to RT, 60 min

2: 43 percent / potassium carbonate / xylene / 5.5 h / Heating

3: iron, ammonium chloride, H₂O / ethanol / 0.5 h / Heating

With copper(I) oxide; hydrogenchloride; ammonium chloride; water; iron; potassium carbonate; sodium nitrite; In ethanol; xylene;
DOI:10.1248/cpb.40.2399

Reference yield:

: 116686-84-1
3'-chloro-4-nitroacetophenone

: 116687-02-6
4'-amino-3'-phenoxyacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / potassium carbonate / xylene / 5.5 h / Heating

2: iron, ammonium chloride, H₂O / ethanol / 0.5 h / Heating

With ammonium chloride; water; iron; potassium carbonate; In ethanol; xylene;
DOI:10.1248/cpb.40.2399