4-methyl-N-(1-phenylhex-5-en-1-yl)benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-(1-phenylhex-5-en-1-yl)benzenesulfonamide
CAS No.:1221972-17-3
Molecular Formula:C₁₉H₂₃NO₂S
Molecular Weight:329.463
Hs Code.:

Synonyms:4-methyl-N-(1-phenylhex-5-en-1-yl)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-N-(1-phenylhex-5-en-1-yl)benzenesulfonamide

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Technology Process of 4-methyl-N-(1-phenylhex-5-en-1-yl)benzenesulfonamide

There total 5 articles about 4-methyl-N-(1-phenylhex-5-en-1-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110775-38-7
1-phenyl-5-hexenyl-1-amine

: 98-59-9
p-toluenesulfonyl chloride

: 1221972-17-3
4-methyl-N-(1-phenylhex-5-en-1-yl)benzenesulfonamide

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/ol100422d

Reference yield:

: 764-59-0
hex-5-en-1-al

: 1221972-17-3
4-methyl-N-(1-phenylhex-5-en-1-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether / 3 h / -78 - 20 °C / Inert atmosphere

2: pyridinium chlorochromate / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

3: ammonium formate / methanol / 20 °C / Inert atmosphere; Molecular sieve

4: sodium carbonate / water; diethyl ether / 20 °C / Inert atmosphere

With ammonium formate; sodium carbonate; pyridinium chlorochromate; In methanol; diethyl ether; dichloromethane; water;
DOI:10.1002/ejoc.201700977

Reference yield:

: 144121-60-8,144121-69-7,65727-70-0
1-phenylhex-5-en-1-ol

: 1221972-17-3
4-methyl-N-(1-phenylhex-5-en-1-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium chlorochromate / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

2: ammonium formate / methanol / 20 °C / Inert atmosphere; Molecular sieve

3: sodium carbonate / water; diethyl ether / 20 °C / Inert atmosphere

With ammonium formate; sodium carbonate; pyridinium chlorochromate; In methanol; diethyl ether; dichloromethane; water;
DOI:10.1002/ejoc.201700977