(1RS)-4-[2-(dimethylamino)-1-(1-hydroxycyclohexyl)ethyl]phenol oxalate

Base Information

Chemical Name:(1RS)-4-[2-(dimethylamino)-1-(1-hydroxycyclohexyl)ethyl]phenol oxalate
CAS No.:1187020-42-3
Molecular Formula:C₂H₂O₄*C₁₆H₂₅NO₂
Molecular Weight:353.415
Hs Code.:

Synonyms:(1RS)-4-[2-(dimethylamino)-1-(1-hydroxycyclohexyl)ethyl]phenol oxalate

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Chemical Property of (1RS)-4-[2-(dimethylamino)-1-(1-hydroxycyclohexyl)ethyl]phenol oxalate

Chemical Property:

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Technology Process of (1RS)-4-[2-(dimethylamino)-1-(1-hydroxycyclohexyl)ethyl]phenol oxalate

There total 6 articles about (1RS)-4-[2-(dimethylamino)-1-(1-hydroxycyclohexyl)ethyl]phenol oxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 144-62-7,97993-78-7
oxalic acid

: 93413-62-8
O-desmethylvenlafaxine

: 1187020-42-3
(1RS)-4-[2-(dimethylamino)-1-(1-hydroxycyclohexyl)ethyl]phenol oxalate

Guidance literature:: In water; acetone; at 0 - 50 ℃;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1187020-42-3
(1RS)-4-[2-(dimethylamino)-1-(1-hydroxycyclohexyl)ethyl]phenol oxalate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium methylate / methanol / 3 h / -5 - 0 °C

1.2: 49 h / -5 °C

2.1: hydrogen; acetic acid / palladium on carbon / 4 h / 43 - 47 °C / 8606.2 Torr

3.1: formic acid / 53 - 57 °C

4.1: sodium methylate; 1-dodecylthiol / polyethylene glycol (PEG-400); methanol / 145 - 150 °C

4.2: 4 h / 105 - 115 °C

4.3: 2 h / 5 - 30 °C

5.1: water; acetone / 26.75 h / 0 - 55 °C

With formic acid; hydrogen; sodium methylate; acetic acid; 1-dodecylthiol; palladium on carbon; In methanol; polyethylene glycol (PEG-400); water; acetone;

Reference yield:

: 104-47-2
p-methoxybenzylnitrile

: 1187020-42-3
(1RS)-4-[2-(dimethylamino)-1-(1-hydroxycyclohexyl)ethyl]phenol oxalate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium methylate / methanol / 3 h / -5 - 0 °C

1.2: 49 h / -5 °C

2.1: hydrogen; acetic acid / palladium on carbon / 4 h / 43 - 47 °C / 8606.2 Torr

3.1: formic acid / 53 - 57 °C

4.1: sodium methylate; 1-dodecylthiol / polyethylene glycol (PEG-400); methanol / 145 - 150 °C

4.2: 4 h / 105 - 115 °C

4.3: 2 h / 5 - 30 °C

5.1: water; acetone / 26.75 h / 0 - 55 °C

With formic acid; hydrogen; sodium methylate; acetic acid; 1-dodecylthiol; palladium on carbon; In methanol; polyethylene glycol (PEG-400); water; acetone;