1-(2,9-dimethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-7-yl)-4-phenethylpiperazin-2-one

Base Information

Chemical Name:1-(2,9-dimethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-7-yl)-4-phenethylpiperazin-2-one
CAS No.:1382774-67-5
Molecular Formula:C₂₅H₃₀N₄O
Molecular Weight:402.539
Hs Code.:

Synonyms:1-(2,9-dimethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-7-yl)-4-phenethylpiperazin-2-one

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Chemical Property of 1-(2,9-dimethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-7-yl)-4-phenethylpiperazin-2-one

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Technology Process of 1-(2,9-dimethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-7-yl)-4-phenethylpiperazin-2-one

There total 6 articles about 1-(2,9-dimethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-7-yl)-4-phenethylpiperazin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1382774-65-3
1-(9-methyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-7-yl)-4-phenethylpiperazin-2-one

: 1382774-67-5
1-(2,9-dimethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-7-yl)-4-phenethylpiperazin-2-one

Guidance literature:: formaldehyd; 1-(9-methyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-7-yl)-4-phenethylpiperazin-2-one; With sodium tris(acetoxy)borohydride; acetic acid; In water; ethyl acetate; for 3h;

With sodium hydrogencarbonate; In water; ethyl acetate;

Reference yield:

: 103-63-9
1-phenyl-2-bromoethane

: 1382774-67-5
1-(2,9-dimethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-7-yl)-4-phenethylpiperazin-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / dimethyl sulfoxide / 5 h / 80 °C

2: caesium carbonate; copper(l) iodide; trans-N,N'-dimethyl-1,2-cyclohexyldiamine / toluene / 16 h / 110 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 1 h

4: acetic acid; sodium tris(acetoxy)borohydride / ethyl acetate; water / 3 h

With trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(l) iodide; sodium tris(acetoxy)borohydride; potassium carbonate; caesium carbonate; acetic acid; trifluoroacetic acid; In dichloromethane; water; dimethyl sulfoxide; ethyl acetate; toluene;

Reference yield:

: 23099-72-1
4-(2-phenylethyl)-2-ketopiperazine

: 1382774-67-5
1-(2,9-dimethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-7-yl)-4-phenethylpiperazin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate; copper(l) iodide; trans-N,N'-dimethyl-1,2-cyclohexyldiamine / toluene / 16 h / 110 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 1 h

3: acetic acid; sodium tris(acetoxy)borohydride / ethyl acetate; water / 3 h

With trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(l) iodide; sodium tris(acetoxy)borohydride; caesium carbonate; acetic acid; trifluoroacetic acid; In dichloromethane; water; ethyl acetate; toluene;