C₂₂H₃₄CuN₂O₂PS

Base Information

Chemical Name:C₂₂H₃₄CuN₂O₂PS
CAS No.:1396176-12-7
Molecular Formula:C₂₂H₃₄CuN₂O₂PS
Molecular Weight:485.11
Hs Code.:

C<sub>22</sub>H<sub>34</sub>CuN<sub>2</sub>O<sub>2</sub>PS

Synonyms:C₂₂H₃₄CuN₂O₂PS

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Chemical Property of C₂₂H₃₄CuN₂O₂PS

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Technology Process of C₂₂H₃₄CuN₂O₂PS

There total 3 articles about C₂₂H₃₄CuN₂O₂PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.6%

: 1357115-05-9
[Cu(μ-Br)(2-di(tert-butyl)phosphinomethyl-6-methylpyridine)]2

: 70-55-3
toluene-4-sulfonamide

: 1396176-12-7
C₂₂H₃₄CuN₂O₂PS

Guidance literature:: [Cu(μ-Br)(2-di(tert-butyl)phosphinomethyl-6-methylpyridine)]2; With potassium tert-butylate; In tetrahydrofuran; diethyl ether; at 20 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

toluene-4-sulfonamide; In tetrahydrofuran; diethyl ether; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c2dt31009k

Reference yield:

: 108-48-5
2,6-dimethylpyridine

: 1396176-12-7
C₂₂H₃₄CuN₂O₂PS

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether / 0 °C / Inert atmosphere; Schlenk technique

1.2: 1 h / -78 °C / Inert atmosphere; Schlenk technique

2.1: diethyl ether / 16 h / 20 °C / Inert atmosphere; Schlenk technique

3.1: potassium tert-butylate / diethyl ether; tetrahydrofuran / 0.08 h / 20 °C / Inert atmosphere; Schlenk technique

3.2: 2 h / Inert atmosphere; Schlenk technique

With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; diethyl ether;
DOI:10.1039/c2dt31009k

Reference yield:

: 13716-10-4
di(tert-butyl)chlorophosphine

: 1396176-12-7
C₂₂H₃₄CuN₂O₂PS

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether / 0 °C / Inert atmosphere; Schlenk technique

1.2: 1 h / -78 °C / Inert atmosphere; Schlenk technique

2.1: diethyl ether / 16 h / 20 °C / Inert atmosphere; Schlenk technique

3.1: potassium tert-butylate / diethyl ether; tetrahydrofuran / 0.08 h / 20 °C / Inert atmosphere; Schlenk technique

3.2: 2 h / Inert atmosphere; Schlenk technique

With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; diethyl ether;
DOI:10.1039/c2dt31009k