S-4-tolyl 4-methoxybenzenesulfinothioate

Base Information

• Chemical Name: S-4-tolyl 4-methoxybenzenesulfinothioate
• CAS No.: 121955-58-6
• Molecular Formula: C₁₄H₁₄O₂S₂
• Molecular Weight: 278.396
• Mol file: 121955-58-6.mol

Synonyms:S-4-tolyl 4-methoxybenzenesulfinothioate

Chemical Property of S-4-tolyl 4-methoxybenzenesulfinothioate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of S-4-tolyl 4-methoxybenzenesulfinothioate

There total 3 articles about S-4-tolyl 4-methoxybenzenesulfinothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

4-methoxybenzenesulfinic acid (1709-60-0) + para-thiocresol (106-45-6) → S-4-tolyl 4-methoxybenzenesulfinothioate (121955-58-6)

Guidance literature:

With Ethyl isocyanoacetate; In dichloromethane; at 20 ℃; for 6h;

DOI:10.1002/adsc.202100915

Reference yield: 20.0%

1-(4-methylphenyldisulfanyl)-4-methoxybenzene (83180-92-1) → S-4-tolyl 4-methoxybenzenesulfinothioate (121955-58-6)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃; for 3h; Inert atmosphere;

DOI:10.1038/aps.2016.170

Reference yield:

→ S-4-tolyl 4-methoxybenzenesulfinothioate (121955-58-6)

Guidance literature:

/BRN= 2697057/;

upstream raw materials:

1-(4-methylphenyldisulfanyl)-4-methoxybenzene

4-methoxybenzenesulfinic acid

para-thiocresol