[4-(3-iodo-5-isopropyl-4-methoxymethoxybenzyl)-3,5-dimethylphenoxy]triisopropylsilane

Base Information

Chemical Name:[4-(3-iodo-5-isopropyl-4-methoxymethoxybenzyl)-3,5-dimethylphenoxy]triisopropylsilane
CAS No.:446312-28-3
Molecular Formula:C₂₉H₄₅IO₃Si
Molecular Weight:596.664
Hs Code.:

Synonyms:[4-(3-iodo-5-isopropyl-4-methoxymethoxybenzyl)-3,5-dimethylphenoxy]triisopropylsilane

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Chemical Property of [4-(3-iodo-5-isopropyl-4-methoxymethoxybenzyl)-3,5-dimethylphenoxy]triisopropylsilane

Chemical Property:

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Technology Process of [4-(3-iodo-5-isopropyl-4-methoxymethoxybenzyl)-3,5-dimethylphenoxy]triisopropylsilane

There total 1 articles about [4-(3-iodo-5-isopropyl-4-methoxymethoxybenzyl)-3,5-dimethylphenoxy]triisopropylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 328236-46-0
3,5-dimethyl-4-(3'-isopropyl-4'-O-methoxymethylbenzyl)-O-triisopropylsilylphenol

: 446312-28-3
[4-(3-iodo-5-isopropyl-4-methoxymethoxybenzyl)-3,5-dimethylphenoxy]triisopropylsilane

Guidance literature:: 3,5-dimethyl-4-(3'-isopropyl-4'-O-methoxymethylbenzyl)-O-triisopropylsilylphenol; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2h;

With N-iodo-succinimide; In tetrahydrofuran; hexane; at 20 ℃; for 5h; Further stages.;
DOI:10.1021/jm0201013

Reference yield:

: 79887-10-8
1-ethynyl-4-(n-pentyl)benzene

: 446312-28-3
[4-(3-iodo-5-isopropyl-4-methoxymethoxybenzyl)-3,5-dimethylphenoxy]triisopropylsilane

: 446312-30-7
triisopropyl-{4-[3-isopropyl-4-methoxymethoxy-5-(4-pentylphenylethynyl)benzyl]-3,5-dimethylphenoxy}silane

Guidance literature:: 1-ethynyl-4-(n-pentyl)benzene; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.5h;

With 9-methoxy-9-BBN; In tetrahydrofuran; hexane; toluene; for 2h;

[4-(3-iodo-5-isopropyl-4-methoxymethoxybenzyl)-3,5-dimethylphenoxy]triisopropylsilane; With bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; hexane; toluene; for 18h; Further stages.; Heating;
DOI:10.1021/jm0201013

Reference yield:

: 536-74-3
phenylacetylene

: 446312-28-3
[4-(3-iodo-5-isopropyl-4-methoxymethoxybenzyl)-3,5-dimethylphenoxy]triisopropylsilane

: 446312-29-4
triisopropyl-[4-(3-isopropyl-4-methoxymethoxy-5-phenylethynylbenzyl)-3,5-dimethylphenoxy]silane

Guidance literature:: phenylacetylene; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.5h;

With 9-methoxy-9-BBN; In tetrahydrofuran; hexane; toluene; for 2h;

[4-(3-iodo-5-isopropyl-4-methoxymethoxybenzyl)-3,5-dimethylphenoxy]triisopropylsilane; With bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; hexane; toluene; for 18h; Further stages.; Heating;
DOI:10.1021/jm0201013