3,5-dimethyl-4-(3'-isopropyl-4'-O-methoxymethylbenzyl)-O-triisopropylsilylphenol

Base Information

Chemical Name:3,5-dimethyl-4-(3'-isopropyl-4'-O-methoxymethylbenzyl)-O-triisopropylsilylphenol
CAS No.:328236-46-0
Molecular Formula:C₂₉H₄₆O₃Si
Molecular Weight:470.768
Hs Code.:

Synonyms:3,5-dimethyl-4-(3'-isopropyl-4'-O-methoxymethylbenzyl)-O-triisopropylsilylphenol

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Chemical Property of 3,5-dimethyl-4-(3'-isopropyl-4'-O-methoxymethylbenzyl)-O-triisopropylsilylphenol

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Technology Process of 3,5-dimethyl-4-(3'-isopropyl-4'-O-methoxymethylbenzyl)-O-triisopropylsilylphenol

There total 11 articles about 3,5-dimethyl-4-(3'-isopropyl-4'-O-methoxymethylbenzyl)-O-triisopropylsilylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 328236-45-9
3,5-dimethyl-4-(3'-isopropyl-4'-O-methoxymethylbenzylhydroxy)-O-triisopropylsilylphenol

: 328236-46-0
3,5-dimethyl-4-(3'-isopropyl-4'-O-methoxymethylbenzyl)-O-triisopropylsilylphenol

Guidance literature:: With hydrogen; acetic acid; palladium 10% on activated carbon; In ethyl acetate; at 20 ℃; for 3h;

Reference yield: 96.0%

: (4-methoxymethoxy-3-iso-propylphenyl)-(2,6-dimethyl-4-triisopropylsilyloxy)-methanol

: 328236-46-0
3,5-dimethyl-4-(3'-isopropyl-4'-O-methoxymethylbenzyl)-O-triisopropylsilylphenol

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In acetic acid; ethyl acetate; at 20 ℃; for 3h;

Reference yield:

: 328236-44-8
2,6-dimethyl-4-(triisopropyl-silanyloxy)-benzaldehyde

: 328236-46-0
3,5-dimethyl-4-(3'-isopropyl-4'-O-methoxymethylbenzyl)-O-triisopropylsilylphenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; pentane / 0.5 h / -78 °C

1.2: 68 percent / tetrahydrofuran; pentane / 7 h / -78 - 20 °C

2.1: 80 percent / AcOH; H₂ / 10 percent Pd/C / ethanol / 12 h / 20 °C / 760 Torr

With n-butyllithium; hydrogen; acetic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; pentane;
DOI:10.1016/S0960-894X(00)00531-X