4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranoside fluoride

Base Information

Chemical Name:4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranoside fluoride
CAS No.:142330-02-7
Molecular Formula:C₅₆H₅₄FNO₁₃
Molecular Weight:968.042
Hs Code.:

Synonyms:4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranoside fluoride

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Chemical Property of 4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranoside fluoride

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Technology Process of 4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranoside fluoride

There total 13 articles about 4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranoside fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 142330-01-6
C₅₆H₅₄ClNO₁₃

: 142330-02-7
4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranoside fluoride

Guidance literature:: With silver fluoride; In acetonitrile;
DOI:10.1246/cl.1992.707

Reference yield: 72.0%

: 4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-D-glucopyranoside

: 142330-02-7
4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranoside fluoride

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1246/bcsj.68.2401

Reference yield:

: 82469-72-5
3,4,6-tri-O-benzoyl-2-(benzoyloximino)-2-deoxy-α-D-arabino-hexopyranosyl bromide

: 142330-02-7
4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranoside fluoride

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / molecular sieves 4 Angsrtoem, silver aluminosilicate / CH₂Cl₂ / 3 h / Ambient temperature

2: BH₃*THF / tetrahydrofuran / 1.) -10 deg C, 0.5 h, 2.) RT, 2 h

3: tetrahydrofuran / 1 h / Ambient temperature

4: 77 percent / CF₃COOH / CH₂Cl₂ / 2 h / 0 °C

5: diethylaminosulfur trifluoride / CH₂Cl₂ / 3 h / Ambient temperature

With borane-THF; diethylamino-sulfur trifluoride; 4 A molecular sieve; silver aluminosilicate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1248/cpb.44.437