Technology Process of C34H42N6O4
There total 1 articles about C34H42N6O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Trimethylenediamine; Wang Resin;
With
1,1'-carbonyldiimidazole;
In
N,N-dimethyl-formamide;
for 24h;
Wang Resin
N-Fmoc L-Phe;
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
for 1h;
Wang Resin
2-ethyl-quinoline-3-carboxylic acid; Fmoc-Pro-OH; 2-(9H-fluoren-9-ylmethoxycarbonylamino)-pent-4-enoic acid;
Further stages;
- Guidance literature:
-
C34H42N6O4; C34H41N6O4Pol;
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride;
In
dichloromethane; 1,2-dichloro-ethane;
Reflux;
With
trifluoroacetic acid;
In
dichloromethane; 1,2-dichloro-ethane;
for 30h;
Overall yield = 64 %; Overall yield = 0.25 g;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / 1,2-dichloro-ethane; dichloromethane / Reflux
1.2: 30 h
2.1: hydrogen; platinum on activated charcoal
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; platinum on activated charcoal; hydrogen;
In
dichloromethane; 1,2-dichloro-ethane;
