Benzoyl chloride, 4-mercapto- (9CI)

Base Information

• Chemical Name: Benzoyl chloride, 4-mercapto- (9CI)
• CAS No.: 110922-46-8
• Molecular Formula: C₇H₅ClOS
• Molecular Weight: 172.635
• Mol file: 110922-46-8.mol

Synonyms:4-Mercaptobenzoylchloride; p-Mercaptobenzoyl chloride

Chemical Property of Benzoyl chloride, 4-mercapto- (9CI)

Chemical Property:

• Boiling Point: 267.5±23.0 °C(Predicted)
• PKA: 4.90±0.10(Predicted)
• PSA: 0.00000
• Density: 1.343±0.06 g/cm3(Predicted)
• LogP: 0.00000

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoyl chloride, 4-mercapto- (9CI)

There total 1 articles about Benzoyl chloride, 4-mercapto- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-mercaptobenzoic acid (1074-36-8) → p-mercaptobenzoyl chloride (110922-46-8)

Guidance literature:

With thionyl chloride; at 70 ℃; for 2h; Inert atmosphere;

DOI:10.1002/cmdc.201800235

Reference yield:

p-mercaptobenzoyl chloride (110922-46-8) → 1-(1H-indol-3-yl)-2-[(4-methyl benzoate)thio]ethanone

Guidance literature:

Multi-step reaction with 2 steps

1: Cooling

2: potassium carbonate / acetone / 5 h / Reflux

With potassium carbonate; In acetone;

DOI:10.1002/cmdc.201800235

Reference yield:

1,10,24,33-tetra-aza<10.1.10.1>paracyclophane (110922-47-9) + p-mercaptobenzoyl chloride (110922-46-8) → bis(N,N'-bis(4-mercaptobenzoyl)-N,N'-octamethylene-4,4'-diaminodiphenylmethane) (110922-48-0)

Guidance literature:

DOI:10.1039/C39870000874

upstream raw materials:

4-mercaptobenzoic acid

Downstream raw materials:

bis(N,N'-bis(4-mercaptobenzoyl)-N,N'-octamethylene-4,4'-diaminodiphenylmethane)

methyl 4-mercaptobenzoate

Refernces