[(C₁₀H₆P(C₆H₅)2)2PdC₆H₅NH₂(CH₂)7CH₃]⁽¹⁺⁾*OSO₂CF₃^(1-)=[(C₁₀H₆P(C₆H₅)2)2PdC₆H₅NH₂(CH₂)7CH₃]OSO₂CF₃

Base Information

• Chemical Name: [(C₁₀H₆P(C₆H₅)2)2PdC₆H₅NH₂(CH₂)7CH₃]⁽¹⁺⁾*OSO₂CF₃^(1-)=[(C₁₀H₆P(C₆H₅)2)2PdC₆H₅NH₂(CH₂)7CH₃]OSO₂CF₃
• CAS No.: 403619-20-5
• Molecular Formula: CF₃O₃S*C₅₈H₅₆NP₂Pd
• Molecular Weight: 1084.53

Synonyms:[(C₁₀H₆P(C₆H₅)2)2PdC₆H₅NH₂(CH₂)7CH₃]⁽¹⁺⁾*OSO₂CF₃^(1-)=[(C₁₀H₆P(C₆H₅)2)2PdC₆H₅NH₂(CH₂)7CH₃]OSO₂CF₃

Chemical Property of [(C₁₀H₆P(C₆H₅)2)2PdC₆H₅NH₂(CH₂)7CH₃]⁽¹⁺⁾*OSO₂CF₃^(1-)=[(C₁₀H₆P(C₆H₅)2)2PdC₆H₅NH₂(CH₂)7CH₃]OSO₂CF₃

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Technology Process of [(C₁₀H₆P(C₆H₅)2)2PdC₆H₅NH₂(CH₂)7CH₃]⁽¹⁺⁾*OSO₂CF₃^(1-)=[(C₁₀H₆P(C₆H₅)2)2PdC₆H₅NH₂(CH₂)7CH₃]OSO₂CF₃

There total 4 articles about [(C₁₀H₆P(C₆H₅)2)2PdC₆H₅NH₂(CH₂)7CH₃]⁽¹⁺⁾*OSO₂CF₃^(1-)=[(C₁₀H₆P(C₆H₅)2)2PdC₆H₅NH₂(CH₂)7CH₃]OSO₂CF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.1%

n-Octylamine (111-86-4) + (C10H6P(C6H5)2)2PdC6H5Br (275801-25-7,1005420-28-9) + silver trifluoromethanesulfonate (2923-28-6) → [(C10H6P(C6H5)2)2PdC6H5NH2(CH2)7CH3](1+)*OSO2CF3(1-)=[(C10H6P(C6H5)2)2PdC6H5NH2(CH2)7CH3]OSO2CF3 (403619-20-5)

Guidance literature:

In toluene; (inert atm.); addn. of amine to a suspn. of palladium complex in toluene, addn. of silver salt, stirring at room temp. for 5 min; decantation, filtration, extn. with toluene, filtration through Celite, concn., layering with pentane, keeping at -34°C overnight, filtration; elem. anal.;

DOI:10.1021/om0108088

Reference yield:

n-Octylamine (111-86-4) + [palladium(S-BINAP)2] + Phenyl triflate (17763-67-6) → [(C10H6P(C6H5)2)2PdC6H5NH2(CH2)7CH3](1+)*OSO2CF3(1-)=[(C10H6P(C6H5)2)2PdC6H5NH2(CH2)7CH3]OSO2CF3 (403619-20-5)

Guidance literature:

With tetrabutylammonium trifluoromethylsulfonate; In tetrahydrofuran; Kinetics;

DOI:10.1021/om0108088

Reference yield:

bromobenzene (108-86-1,52753-63-6) → [(C10H6P(C6H5)2)2PdC6H5NH2(CH2)7CH3](1+)*OSO2CF3(1-)=[(C10H6P(C6H5)2)2PdC6H5NH2(CH2)7CH3]OSO2CF3 (403619-20-5)

Guidance literature:

Multi-step reaction with 2 steps

1: not given

2: toluene

In toluene;

DOI:10.1021/om0108088

upstream raw materials:

n-Octylamine

(C₁₀H₆P(C₆H₅)2)2PdC₆H₅Br

silver trifluoromethanesulfonate

Phenyl triflate

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