(Z)-2-(4-fluorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

Base Information

Chemical Name:(Z)-2-(4-fluorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate
CAS No.:1311272-09-9
Molecular Formula:C₂₆H₂₇FO₄
Molecular Weight:422.496
Hs Code.:

Synonyms:(Z)-2-(4-fluorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(4-fluorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

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Technology Process of (Z)-2-(4-fluorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

There total 6 articles about (Z)-2-(4-fluorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.3%

: 38460-95-6
undec-10-enoyl chloride

: 1261274-04-7
(Z)-5-hydroxy-2-(4-fluorobenzylidene)benzofuran-3(2H)-one

: 1311272-09-9
(Z)-2-(4-fluorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

Guidance literature:: With pyridine; In dichloromethane; Reflux;
DOI:10.1016/j.bmc.2011.03.063

Reference yield:

: 1311272-36-2
2'-hydroxy-5'-(methoxymethoxy)-4-fluorochalcone

: 1311272-09-9
(Z)-2-(4-fluorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; mercury(II) diacetate / 1 h / 110 °C

2: hydrogenchloride; water / methanol / 0.5 h / Reflux

3: pyridine / dichloromethane / Reflux

With pyridine; hydrogenchloride; mercury(II) diacetate; water; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.03.063

Reference yield:

: 1311272-29-3
(Z)-2-(4-fluorobenzylidene)-5-(methoxymethoxy)benzo[b]furan-3-one

: 1311272-09-9
(Z)-2-(4-fluorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / methanol / 0.5 h / Reflux

2: pyridine / dichloromethane / Reflux

With pyridine; hydrogenchloride; water; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.03.063