C₃₀H₃₉NO₉Se

Base Information

Chemical Name:C₃₀H₃₉NO₉Se
CAS No.:114250-82-7
Molecular Formula:C₃₀H₃₉NO₉Se
Molecular Weight:636.601
Hs Code.:

C<sub>30</sub>H<sub>39</sub>NO<sub>9</sub>Se

Synonyms:C₃₀H₃₉NO₉Se

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Chemical Property of C₃₀H₃₉NO₉Se

Chemical Property:

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Technology Process of C₃₀H₃₉NO₉Se

There total 25 articles about C₃₀H₃₉NO₉Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60078-92-4,14393-38-5
2,4,4-trimethyl-3-formyl-2-cyclohexen-1-ol

: 114250-82-7
C₃₀H₃₉NO₉Se

Guidance literature:: Multi-step reaction with 24 steps

1: Wittig methylenation

2: 72 percent / CHCl₃ / 30 h / 23 °C

3: BF₃*Et₂O / -35 deg C, 1 h, 0 deg C, 15 min

4: DBN / 0.75 h / 23 °C

5: O₂ / 0.1percent methylene blue / CHCl₃ / 144 h / 0 °C / Irradiation

6: 97 percent / AlHg / tetrahydrofuran; H₂O / 0.17 h / 23 °C

7: 85 percent / DMAP / 1,2-dichloro-ethane / 2 h / 50 °C

8: 1.) pyridinium chlorochromate, 2.) AlHg / 1.) 1,2-dichloroethane, 80 to 90 deg C, 5 h, 2.) THF - H₂O, 20 deg C, 18 min

9: 99 percent / diethyl ether

10: diisobutylaluminumhydride / toluene / 1.25 h / -78 °C

11: tert-butyl hydroperoxide / Mo(CO)6 / benzene / 1 h / 68 °C

12: KOH / methanol / 0.17 h / 23 °C

13: 99 percent / tosic acid / acetone / 1.5 h / 23 °C

14: 80 percent / tetrahydrofuran / 0 °C

15: 60 percent / 2,6-lutidine, silver triflate / CH₂Cl₂ / 23 °C

16: 1.) K₂CO₃, 2.) oxalic acid / 1.) THF - ethylene glycol, 23 deg C, 2 h, 2.) water - aceton, 60 deg C, 7 h

17: imidazole / dimethylformamide / 0.5 h / 23 °C

18: 82 percent / 1.) thallous ethoxide / 1.) 23 deg C, 30 min, 2.) -78 to 45 deg C, 1 h

19: 63 percent / O₂ / methylene blue / CHCl₃ / 5 h / 10 °C / Irradiation

20: 80 percent / NaOCH₃, Bu₃P / ethanol / 2.5 h / 0 °C

21: acetic acid / 23 h / 100 - 105 °C / in sealed tube

22: 85 percent / BF₃*Et₂O / diethyl ether / -78deg C, 4 h, -50 deg C, 15 min

23: 2percent HF / acetonitrile; H₂O / 0.25 h / 0 °C

24: n-Bu₃P / tetrahydrofuran / 2 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; tert.-butylhydroperoxide; dmap; potassium hydroxide; tributylphosphine; aluminium amalgam; 2,6-dichloro-benzonitrile; boron trifluoride diethyl etherate; hydrogen fluoride; oxygen; sodium methylate; silver trifluoromethanesulfonate; thallium (I) ethoxide; oxalic acid; diisobutylaluminium hydride; potassium carbonate; pyridinium chlorochromate; hexacarbonyl molybdenum; methylene blue; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; chloroform; water; acetic acid; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; benzene;
DOI:10.1021/ja00219a059

Reference yield:

: 14398-36-8
(3E)-4-[(S)-2,6,6-trimethylcyclohex-2-enyl]but-3-en-2-one

: 114250-82-7
C₃₀H₃₉NO₉Se

Guidance literature:: Multi-step reaction with 25 steps

2: Wittig methylenation

3: 72 percent / CHCl₃ / 30 h / 23 °C

4: BF₃*Et₂O / -35 deg C, 1 h, 0 deg C, 15 min

5: DBN / 0.75 h / 23 °C

6: O₂ / 0.1percent methylene blue / CHCl₃ / 144 h / 0 °C / Irradiation

7: 97 percent / AlHg / tetrahydrofuran; H₂O / 0.17 h / 23 °C

8: 85 percent / DMAP / 1,2-dichloro-ethane / 2 h / 50 °C

9: 1.) pyridinium chlorochromate, 2.) AlHg / 1.) 1,2-dichloroethane, 80 to 90 deg C, 5 h, 2.) THF - H₂O, 20 deg C, 18 min

10: 99 percent / diethyl ether

11: diisobutylaluminumhydride / toluene / 1.25 h / -78 °C

12: tert-butyl hydroperoxide / Mo(CO)6 / benzene / 1 h / 68 °C

13: KOH / methanol / 0.17 h / 23 °C

14: 99 percent / tosic acid / acetone / 1.5 h / 23 °C

15: 80 percent / tetrahydrofuran / 0 °C

16: 60 percent / 2,6-lutidine, silver triflate / CH₂Cl₂ / 23 °C

17: 1.) K₂CO₃, 2.) oxalic acid / 1.) THF - ethylene glycol, 23 deg C, 2 h, 2.) water - aceton, 60 deg C, 7 h

18: imidazole / dimethylformamide / 0.5 h / 23 °C

19: 82 percent / 1.) thallous ethoxide / 1.) 23 deg C, 30 min, 2.) -78 to 45 deg C, 1 h

20: 63 percent / O₂ / methylene blue / CHCl₃ / 5 h / 10 °C / Irradiation

21: 80 percent / NaOCH₃, Bu₃P / ethanol / 2.5 h / 0 °C

22: acetic acid / 23 h / 100 - 105 °C / in sealed tube

23: 85 percent / BF₃*Et₂O / diethyl ether / -78deg C, 4 h, -50 deg C, 15 min

24: 2percent HF / acetonitrile; H₂O / 0.25 h / 0 °C

25: n-Bu₃P / tetrahydrofuran / 2 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; tert.-butylhydroperoxide; dmap; potassium hydroxide; tributylphosphine; aluminium amalgam; 2,6-dichloro-benzonitrile; boron trifluoride diethyl etherate; hydrogen fluoride; oxygen; sodium methylate; silver trifluoromethanesulfonate; thallium (I) ethoxide; oxalic acid; diisobutylaluminium hydride; potassium carbonate; pyridinium chlorochromate; hexacarbonyl molybdenum; methylene blue; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; chloroform; water; acetic acid; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; benzene;
DOI:10.1021/ja00219a059

Reference yield:

: 128442-09-1
(2aβ,5β,5aα,8aβ,8bβ)-2a,5,5a,6,7,8,8a,8b-Octahydro-5-hydroxy-3,6,6,8b-tetramethyl-2H-naphtho<1,8-bc>furan-2-one

: 114250-82-7
C₃₀H₃₉NO₉Se

Guidance literature:: Multi-step reaction with 14 steps

1: tert-butyl hydroperoxide / Mo(CO)6 / benzene / 1 h / 68 °C

2: KOH / methanol / 0.17 h / 23 °C

3: 99 percent / tosic acid / acetone / 1.5 h / 23 °C

4: 80 percent / tetrahydrofuran / 0 °C

5: 60 percent / 2,6-lutidine, silver triflate / CH₂Cl₂ / 23 °C

6: 1.) K₂CO₃, 2.) oxalic acid / 1.) THF - ethylene glycol, 23 deg C, 2 h, 2.) water - aceton, 60 deg C, 7 h

7: imidazole / dimethylformamide / 0.5 h / 23 °C

8: 82 percent / 1.) thallous ethoxide / 1.) 23 deg C, 30 min, 2.) -78 to 45 deg C, 1 h

9: 63 percent / O₂ / methylene blue / CHCl₃ / 5 h / 10 °C / Irradiation

10: 80 percent / NaOCH₃, Bu₃P / ethanol / 2.5 h / 0 °C

11: acetic acid / 23 h / 100 - 105 °C / in sealed tube

12: 85 percent / BF₃*Et₂O / diethyl ether / -78deg C, 4 h, -50 deg C, 15 min

13: 2percent HF / acetonitrile; H₂O / 0.25 h / 0 °C

14: n-Bu₃P / tetrahydrofuran / 2 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; tert.-butylhydroperoxide; potassium hydroxide; tributylphosphine; boron trifluoride diethyl etherate; hydrogen fluoride; oxygen; sodium methylate; silver trifluoromethanesulfonate; thallium (I) ethoxide; oxalic acid; potassium carbonate; hexacarbonyl molybdenum; methylene blue; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; chloroform; water; acetic acid; N,N-dimethyl-formamide; acetone; acetonitrile; benzene;
DOI:10.1021/ja00219a059