9-(4-hydroxyphenyl)-9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene

Base Information

Chemical Name:9-(4-hydroxyphenyl)-9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene
CAS No.:1446220-02-5
Molecular Formula:C₃₈H₃₆O₄
Molecular Weight:556.701
Hs Code.:

Synonyms:9-(4-hydroxyphenyl)-9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene

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Chemical Property of 9-(4-hydroxyphenyl)-9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene

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Technology Process of 9-(4-hydroxyphenyl)-9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene

There total 1 articles about 9-(4-hydroxyphenyl)-9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 625122-37-4
2-methyl-2-adamantyl bromoacetate

: 3236-71-3
9,9-bis(4-hydroxyphenyl)fluorene

: 1446220-02-5
9-(4-hydroxyphenyl)-9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetonitrile; at 60 ℃;
DOI:10.1002/pola.26575

Reference yield: 82.0%

: 1446220-02-5
9-(4-hydroxyphenyl)-9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene

: 79-08-3
bromoacetic acid

: 1446220-04-7
9-(4-hydroxycarbonylmethoxyphenyl)-9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene

Guidance literature:: 9-(4-hydroxyphenyl)-9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

bromoacetic acid; In tetrahydrofuran; at 0 ℃; for 24h; Reflux;
DOI:10.1002/pola.26575

Reference yield:

: 1446220-02-5
9-(4-hydroxyphenyl)-9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene

: 1446220-06-9
sodium 4-(9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene-9-yl)phenoxyacetyl-2,3,5,6-tetrafluorobenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C

1.2: 24 h / 0 °C / Reflux

2.1: dicyclohexyl-carbodiimide / acetone; N,N-dimethyl-formamide / 50 °C

With sodium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;
DOI:10.1002/pola.26575