sodium 4-(9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene-9-yl)phenoxyacetyl-2,3,5,6-tetrafluorobenzenesulfonate

Base Information

Chemical Name:sodium 4-(9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene-9-yl)phenoxyacetyl-2,3,5,6-tetrafluorobenzenesulfonate
CAS No.:1446220-06-9
Molecular Formula:C₄₆H₃₇F₄O₉S*Na
Molecular Weight:864.844
Hs Code.:

Synonyms:sodium 4-(9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene-9-yl)phenoxyacetyl-2,3,5,6-tetrafluorobenzenesulfonate

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Chemical Property of sodium 4-(9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene-9-yl)phenoxyacetyl-2,3,5,6-tetrafluorobenzenesulfonate

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Technology Process of sodium 4-(9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene-9-yl)phenoxyacetyl-2,3,5,6-tetrafluorobenzenesulfonate

There total 4 articles about sodium 4-(9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene-9-yl)phenoxyacetyl-2,3,5,6-tetrafluorobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1446220-04-7
9-(4-hydroxycarbonylmethoxyphenyl)-9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene

: 2,3,5,6-tetrafluoro-4-hydroxybenzene sulfonic acid sodium salt

: 1446220-06-9
sodium 4-(9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene-9-yl)phenoxyacetyl-2,3,5,6-tetrafluorobenzenesulfonate

Guidance literature:: With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; acetone; at 50 ℃;
DOI:10.1002/pola.26575

Reference yield:

: 625122-37-4
2-methyl-2-adamantyl bromoacetate

: 1446220-06-9
sodium 4-(9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene-9-yl)phenoxyacetyl-2,3,5,6-tetrafluorobenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; 18-crown-6 ether / acetonitrile / 60 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C

2.2: 24 h / 0 °C / Reflux

3.1: dicyclohexyl-carbodiimide / acetone; N,N-dimethyl-formamide / 50 °C

With 18-crown-6 ether; sodium hydride; potassium carbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1002/pola.26575

Reference yield:

: 1446220-02-5
9-(4-hydroxyphenyl)-9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene

: 1446220-06-9
sodium 4-(9-(4-(2-methyl-2-adamantyloxycarbonylmethyloxy)phenyl)fluorene-9-yl)phenoxyacetyl-2,3,5,6-tetrafluorobenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C

1.2: 24 h / 0 °C / Reflux

2.1: dicyclohexyl-carbodiimide / acetone; N,N-dimethyl-formamide / 50 °C

With sodium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;
DOI:10.1002/pola.26575