D-Alanine, N-D-alanyl-, labeled with carbon-14 (9CI)

Base Information

• Chemical Name: D-Alanine, N-D-alanyl-, labeled with carbon-14 (9CI)
• CAS No.: 110652-05-6
• Molecular Formula: C₆H₁₂N₂O₃
• Molecular Weight: 160.173
• Mol file: 110652-05-6.mol

Synonyms:D-Alanine, N-D-alanyl-, labeled with carbon-14 (9CI)

Chemical Property of D-Alanine, N-D-alanyl-, labeled with carbon-14 (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of D-Alanine, N-D-alanyl-, labeled with carbon-14 (9CI)

There total 69 articles about D-Alanine, N-D-alanyl-, labeled with carbon-14 (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-alanine-L-alanine-p-nitroanilide (57282-69-6,115846-28-1,115846-37-2) → di-L-alanine (1948-31-8,110652-05-6,210687-33-5,2392-61-2) + 4-nitro-aniline (100-01-6,104810-17-5)

Guidance literature:

at 37 ℃; for 0.166667h; 0.1 M Tris HCl buffer pH 8.0, X-prolyl dipeptidyl aminopeptidase from Lactococcus lactis subsp. cremoris nTR;

DOI:10.1271/bbb.56.704

Reference yield:

N-pyruvoyl-alanine (2392-63-4,188300-91-6,877036-29-8) + water (7732-18-5) + phenylglycin (2835-06-5) → DL-α-alanylalanine (1115-78-2,1948-31-8,2867-20-1,3695-80-5,56271-29-5,59247-16-4,90580-65-7,90760-70-6,99265-26-6,923-16-0,110652-05-6,210687-33-5,2392-61-2) + carbon dioxide (124-38-9,18923-20-1) + benzaldehyde (100-52-7)

Guidance literature:

Reference yield:

L-alanin (56-41-7,25191-17-7,18875-37-1) + (S,S)-N,N'-bis(1-carboxyethyl)urea (98337-25-8) → (R)-2-((S)-2-Amino-propionylamino)-propionic acid (3695-80-5,110652-05-6,210687-33-5,2392-61-2) + di-L-alanine (1948-31-8,110652-05-6,210687-33-5,2392-61-2) + L-ala-L-ala-L-ala (5874-90-8)

Guidance literature:

With carbon dioxide; sodium hydrogencarbonate; at 80 ℃; for 840h; pH=7.1;

DOI:10.1021/ja061339+

upstream raw materials:

DL-2-(2-hydroxyimino-propionylamino)-propionic acid

N-(2-bromo-propionyl)-alanine

cyclo(-DL-Ala-DL-Ala-)

AlaOEt

Downstream raw materials:

(S)-methyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

adenosine 2',3'-cyclic monophosphate

C₁₈H₂₅N₃O₆

D-alanyl-D-alanine methyl ester hydrochloride

Refernces

• 1、 Munegumi, Toratane,Fujimoto, Takeshi,Michiotakada,Nozominagashima. "Epimerization of cyclic alanyl-alanine in basic solutions". . p. 23 - 30. Retrieved 2014.
• 2、 Ellenbogen. "-". . . Retrieved 1956.
• 3、 Ying, Jianxi,Chen, Peng,Wu, Yile,Yang, Xu,Yan, Kaili,Xu, Pengxiang,Zhao, Yufen. "Effect of high hydrostatic pressure on prebiotic peptide synthesis". . p. 367 - 370. Retrieved 2019.
• 4、 Fujimoto, Chikako,Shinozaki, Ayako,Mimura, Koichi,Nishida, Tamihito,Gotou, Hirotada,Komatsu, Kazuki,Kagi, Hiroyuki. "Pressure-induced oligomerization of alanine at 25 °C". . p. 13358 - 13361. Retrieved 2015.
• 5、 Li,N.C. et al.. "-". . p. 3737 - 3739. Retrieved 1960.
• 6、 Klepel, Florian,Ravoo, Bart Jan. "A dynamic combinatorial library for biomimetic recognition of dipeptides in water". supporting information. p. 1588 - 1595. Retrieved 2020/09/16.