DM-4107

Base Information

Chemical Name:DM-4107
CAS No.:1346599-75-4
Molecular Formula:C₂₆H₂₅ClN₂O₅
Molecular Weight:480.948
Hs Code.:

Synonyms:DM-4107

Suppliers and Price of DM-4107

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Tolvaptanγ-HydroxybutanoicAcidImpurity
10mg
$ 2385.00

Total 6 raw suppliers

Chemical Property of DM-4107

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Tolvaptanγ-HydroxybutanoicAcidImpurity ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses A Tolvaptan (T536650) Impurity.

Technology Process of DM-4107

There total 10 articles about DM-4107 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1346599-56-1
DM-4103

: 1346599-75-4
DM-4107

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃;
DOI:10.1016/j.cclet.2012.11.001

Reference yield:

: 62903-14-4
4-(3-chlorophenyl)-4-oxobutyric acid

: 1346599-75-4
DM-4107

Guidance literature:: Multi-step reaction with 8 steps

1: sulfuric acid; nitric acid / -20 °C

2: sulfuric acid / Reflux

3: hydrogen; 1% platinum on charcoal / ethanol

4: pyridine / dichloromethane

5: hydrogen; 1% platinum on charcoal / ethanol / 20 °C

6: triethylamine / dichloromethane / 20 °C

7: sodium hydroxide / methanol / 20 °C

8: sodium tetrahydroborate / methanol / 20 °C

With pyridine; sodium tetrahydroborate; sulfuric acid; 1% platinum on charcoal; hydrogen; nitric acid; triethylamine; sodium hydroxide; In methanol; ethanol; dichloromethane;
DOI:10.1016/j.cclet.2012.11.001

Reference yield:

: 1417520-48-9
C₁₁H₁₀ClNO₅

: 1346599-75-4
DM-4107

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogen; 1% platinum on charcoal / ethanol

2: pyridine / dichloromethane

3: hydrogen; 1% platinum on charcoal / ethanol / 20 °C

4: triethylamine / dichloromethane / 20 °C

5: sodium hydroxide / methanol / 20 °C

6: sodium tetrahydroborate / methanol / 20 °C

With pyridine; sodium tetrahydroborate; 1% platinum on charcoal; hydrogen; triethylamine; sodium hydroxide; In methanol; ethanol; dichloromethane;
DOI:10.1016/j.cclet.2012.11.001