(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (1R,4R,5S,7R,8R)-8-acetoxy-2-benzyl-4-(methoxymethoxy)-3-oxo-7-[(trifluoromethyl)sulfonyloxy]-2-azabicyclo[2.2.2]octane-5-carboxylate

Base Information Edit

Chemical Name:(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (1R,4R,5S,7R,8R)-8-acetoxy-2-benzyl-4-(methoxymethoxy)-3-oxo-7-[(trifluoromethyl)sulfonyloxy]-2-azabicyclo[2.2.2]octane-5-carboxylate
CAS No.:660849-30-9
Molecular Formula:C₃₆H₄₄F₃NO₁₀S
Molecular Weight:739.807
Hs Code.:
Mol file:660849-30-9.mol

(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (1R,4R,5S,7R,8R)-8-acetoxy-2-benzyl-4-(methoxymethoxy)-3-oxo-7-[(trifluoromethyl)sulfonyloxy]-2-azabicyclo[2.2.2]octane-5-carboxylate

Synonyms:(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (1R,4R,5S,7R,8R)-8-acetoxy-2-benzyl-4-(methoxymethoxy)-3-oxo-7-[(trifluoromethyl)sulfonyloxy]-2-azabicyclo[2.2.2]octane-5-carboxylate

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Chemical Property of (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (1R,4R,5S,7R,8R)-8-acetoxy-2-benzyl-4-(methoxymethoxy)-3-oxo-7-[(trifluoromethyl)sulfonyloxy]-2-azabicyclo[2.2.2]octane-5-carboxylate Edit

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Technology Process of (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (1R,4R,5S,7R,8R)-8-acetoxy-2-benzyl-4-(methoxymethoxy)-3-oxo-7-[(trifluoromethyl)sulfonyloxy]-2-azabicyclo[2.2.2]octane-5-carboxylate

There total 1 articles about (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (1R,4R,5S,7R,8R)-8-acetoxy-2-benzyl-4-(methoxymethoxy)-3-oxo-7-[(trifluoromethyl)sulfonyloxy]-2-azabicyclo[2.2.2]octane-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 108-24-7
acetic anhydride

: 660849-28-5
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (1R,4R,5S,7R,8R)-2-benzyl-7,8-dihydroxy-4-(methoxymethoxy)-3-oxo-2-azabicyclo[2.2.2]octane-5-carboxylate

: 660849-30-9
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (1R,4R,5S,7R,8R)-8-acetoxy-2-benzyl-4-(methoxymethoxy)-3-oxo-7-[(trifluoromethyl)sulfonyloxy]-2-azabicyclo[2.2.2]octane-5-carboxylate

: (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (1R,4R,5S,7R,8R)-2-benzyl-4-(methoxymethoxy)-3-oxo-7,8-bis[(trifluoromethyl)sulfonyloxy]-2-azabicyclo[2.2.2]octane-5-carboxylate

Guidance literature:: trifluoromethylsulfonic anhydride; (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (1R,4R,5S,7R,8R)-2-benzyl-7,8-dihydroxy-4-(methoxymethoxy)-3-oxo-2-azabicyclo[2.2.2]octane-5-carboxylate; In pyridine; dichloromethane; at 24 ℃; for 12h;

acetic anhydride; In pyridine; dichloromethane; for 4h; under 25 Torr;
DOI:10.1002/hlca.200390321