3-{4-[2-(4'-formyl-5'-iodo-4,2'-dimethoxybiphen-2-yl)ethyl]phenoxy}-4-methoxybenzaldehyde

Base Information

Chemical Name:3-{4-[2-(4'-formyl-5'-iodo-4,2'-dimethoxybiphen-2-yl)ethyl]phenoxy}-4-methoxybenzaldehyde
CAS No.:863408-30-4
Molecular Formula:C₃₁H₂₇IO₆
Molecular Weight:622.456
Hs Code.:

Synonyms:3-{4-[2-(4'-formyl-5'-iodo-4,2'-dimethoxybiphen-2-yl)ethyl]phenoxy}-4-methoxybenzaldehyde

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Chemical Property of 3-{4-[2-(4'-formyl-5'-iodo-4,2'-dimethoxybiphen-2-yl)ethyl]phenoxy}-4-methoxybenzaldehyde

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Technology Process of 3-{4-[2-(4'-formyl-5'-iodo-4,2'-dimethoxybiphen-2-yl)ethyl]phenoxy}-4-methoxybenzaldehyde

There total 4 articles about 3-{4-[2-(4'-formyl-5'-iodo-4,2'-dimethoxybiphen-2-yl)ethyl]phenoxy}-4-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 863408-34-8
4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}ethyl)-5-iodo-2,4'-dimethoxybiphenyl

: 863408-30-4
3-{4-[2-(4'-formyl-5'-iodo-4,2'-dimethoxybiphen-2-yl)ethyl]phenoxy}-4-methoxybenzaldehyde

Guidance literature:: With water; pyridinium p-toluenesulfonate; In acetone; for 18h; Heating;
DOI:10.1002/anie.200500466

Reference yield:

: 4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}vinyl)-4'-methoxybiphenyl-2-ol

: 863408-30-4
3-{4-[2-(4'-formyl-5'-iodo-4,2'-dimethoxybiphen-2-yl)ethyl]phenoxy}-4-methoxybenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / hydrogen; triethylamine / platinum oxide / ethanol / 18 h / 20 °C

2: 73 percent / sodium iodide; NaOH; NaOCl / methanol; H₂O / 3 h

3: 88 percent / potassium carbonate / acetone / 18 h / 20 °C

4: 83 percent / water; pyridinium p-toluenesulfonate / acetone / 18 h / Heating

With sodium hydroxide; sodium hypochlorite; water; hydrogen; pyridinium p-toluenesulfonate; potassium carbonate; triethylamine; sodium iodide; platinum(IV) oxide; In methanol; ethanol; water; acetone;
DOI:10.1002/anie.200500466

Reference yield:

: 863408-28-0
4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}ethyl)-4'-methoxybiphenyl-2-ol

: 863408-30-4
3-{4-[2-(4'-formyl-5'-iodo-4,2'-dimethoxybiphen-2-yl)ethyl]phenoxy}-4-methoxybenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / sodium iodide; NaOH; NaOCl / methanol; H₂O / 3 h

2: 88 percent / potassium carbonate / acetone / 18 h / 20 °C

3: 83 percent / water; pyridinium p-toluenesulfonate / acetone / 18 h / Heating

With sodium hydroxide; sodium hypochlorite; water; pyridinium p-toluenesulfonate; potassium carbonate; sodium iodide; In methanol; water; acetone;
DOI:10.1002/anie.200500466