4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}ethyl)-5-iodo-2,4'-dimethoxybiphenyl

Base Information

Chemical Name:4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}ethyl)-5-iodo-2,4'-dimethoxybiphenyl
CAS No.:863408-34-8
Molecular Formula:C₄₁H₄₇IO₈
Molecular Weight:794.724
Hs Code.:

Synonyms:4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}ethyl)-5-iodo-2,4'-dimethoxybiphenyl

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Chemical Property of 4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}ethyl)-5-iodo-2,4'-dimethoxybiphenyl

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Technology Process of 4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}ethyl)-5-iodo-2,4'-dimethoxybiphenyl

There total 3 articles about 4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}ethyl)-5-iodo-2,4'-dimethoxybiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 863408-29-1
4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}ethyl)-5-iodo-4'-methoxybiphenyl-2-ol

: 74-88-4
methyl iodide

: 863408-34-8
4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}ethyl)-5-iodo-2,4'-dimethoxybiphenyl

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 18h;
DOI:10.1002/anie.200500466

Reference yield:

: 4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}vinyl)-4'-methoxybiphenyl-2-ol

: 863408-34-8
4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}ethyl)-5-iodo-2,4'-dimethoxybiphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / hydrogen; triethylamine / platinum oxide / ethanol / 18 h / 20 °C

2: 73 percent / sodium iodide; NaOH; NaOCl / methanol; H₂O / 3 h

3: 88 percent / potassium carbonate / acetone / 18 h / 20 °C

With sodium hydroxide; sodium hypochlorite; hydrogen; potassium carbonate; triethylamine; sodium iodide; platinum(IV) oxide; In methanol; ethanol; water; acetone;
DOI:10.1002/anie.200500466

Reference yield:

: 863408-28-0
4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}ethyl)-4'-methoxybiphenyl-2-ol

: 863408-34-8
4-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2'-(2-{4-[5-(5,5-dimethyl-[1,3]dioxolan-2-yl)-2-methoxyphenoxy]phenyl}ethyl)-5-iodo-2,4'-dimethoxybiphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / sodium iodide; NaOH; NaOCl / methanol; H₂O / 3 h

2: 88 percent / potassium carbonate / acetone / 18 h / 20 °C

With sodium hydroxide; sodium hypochlorite; potassium carbonate; sodium iodide; In methanol; water; acetone;
DOI:10.1002/anie.200500466