Technology Process of C40H29BrN2O3
There total 5 articles about C40H29BrN2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
phosphorus tribromide;
In
dichloromethane;
at 0 ℃;
for 5h;
DOI:10.1021/ja710803p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane
2: potassium carbonate; potassium iodide / acetonitrile / 24 h / Reflux
3: phosphorus tribromide / dichloromethane / 5 h / 0 °C
With
N-Bromosuccinimide; phosphorus tribromide; potassium carbonate; potassium iodide; dibenzoyl peroxide;
In
tetrachloromethane; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium phosphate; copper(l) iodide; 2(R),3(S)-diaminocyclohexane / toluene
2: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane
3: potassium carbonate; potassium iodide / acetonitrile / 24 h / Reflux
4: phosphorus tribromide / dichloromethane / 5 h / 0 °C
With
potassium phosphate; N-Bromosuccinimide; copper(l) iodide; phosphorus tribromide; 2(R),3(S)-diaminocyclohexane; potassium carbonate; potassium iodide; dibenzoyl peroxide;
In
tetrachloromethane; dichloromethane; toluene; acetonitrile;