C₃₂H₂₂O

Base Information

Chemical Name:C₃₂H₂₂O
CAS No.:579472-33-6
Molecular Formula:C₃₂H₂₂O
Molecular Weight:422.526
Hs Code.:

Synonyms:C₃₂H₂₂O

Suppliers and Price of C₃₂H₂₂O

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₂H₂₂O

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₂H₂₂O

There total 5 articles about C₃₂H₂₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 579472-32-5
C₃₂H₂₄Br₂O

: 579472-33-6
C₃₂H₂₂O

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl acetamide; at 160 ℃; for 12h;
DOI:10.1021/ma048728d

Reference yield:

: C₂₄H₁₇Br₂O⁽¹⁺⁾*BF₄^(1-)

: 579472-33-6
C₃₂H₂₂O

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / acetic anhydride / 2 h / 150 °C

2: 42 percent / PdCl₂(PPh₃)2; 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-acetamide / 12 h / 160 °C

With bis-triphenylphosphine-palladium(II) chloride; acetic anhydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl acetamide;
DOI:10.1021/ma048728d

Reference yield:

: 2142-69-0
2-bromophenyl methyl ketone

: 579472-33-6
C₃₂H₂₂O

Guidance literature:: Multi-step reaction with 4 steps

1: 33 percent / sodium hydroxide / 0.42 h

2: 89 percent / chalcone; BF₃*Et₂O / 2 h / 100 °C

3: 37 percent / acetic anhydride / 2 h / 150 °C

4: 41.8 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene; PdCl₂(PPh₃)2 / N,N-dimethyl-acetamide / 12 h / 160 °C

With bis-triphenylphosphine-palladium(II) chloride; sodium hydroxide; boron trifluoride diethyl etherate; acetic anhydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; benzalacetophenone; In N,N-dimethyl acetamide;
DOI:10.1021/ol034626g