2-amino-5-[2-amino-1-(phenylsulfonyl)-1H-benzimidazol-6-yl]-N-phenyl-3-pyridinesulfonamide

Base Information

Chemical Name:2-amino-5-[2-amino-1-(phenylsulfonyl)-1H-benzimidazol-6-yl]-N-phenyl-3-pyridinesulfonamide
CAS No.:1416333-43-1
Molecular Formula:C₂₄H₂₀N₆O₄S₂
Molecular Weight:520.593
Hs Code.:

Synonyms:2-amino-5-[2-amino-1-(phenylsulfonyl)-1H-benzimidazol-6-yl]-N-phenyl-3-pyridinesulfonamide

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Chemical Property of 2-amino-5-[2-amino-1-(phenylsulfonyl)-1H-benzimidazol-6-yl]-N-phenyl-3-pyridinesulfonamide

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Technology Process of 2-amino-5-[2-amino-1-(phenylsulfonyl)-1H-benzimidazol-6-yl]-N-phenyl-3-pyridinesulfonamide

There total 4 articles about 2-amino-5-[2-amino-1-(phenylsulfonyl)-1H-benzimidazol-6-yl]-N-phenyl-3-pyridinesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.67%

: 1366132-05-9
2-amino-N-phenyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine-3-sulfonamide

: 1416337-05-7
6-iodo-1-(phenylsulfonyl)-1H-benzo[d]imidazol-2-amine

: 1416333-43-1
2-amino-5-[2-amino-1-(phenylsulfonyl)-1H-benzimidazol-6-yl]-N-phenyl-3-pyridinesulfonamide

Guidance literature:: With potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; water; at 50 ℃;

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 1416333-43-1
2-amino-5-[2-amino-1-(phenylsulfonyl)-1H-benzimidazol-6-yl]-N-phenyl-3-pyridinesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile; water / 4 h / 20 °C

2: N-iodo-succinimide / acetic acid / 16 h / 55 °C

3: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 50 °C

With N-iodo-succinimide; potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; water; acetic acid; acetonitrile; 3: Suzuki Coupling;

Reference yield:

: 934-32-7
1H-benzimidazol-2-amine

: 1416333-43-1
2-amino-5-[2-amino-1-(phenylsulfonyl)-1H-benzimidazol-6-yl]-N-phenyl-3-pyridinesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile; water / 4 h / 20 °C

2: N-iodo-succinimide / acetic acid / 16 h / 55 °C

3: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 50 °C

With N-iodo-succinimide; potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; water; acetic acid; acetonitrile; 3: Suzuki Coupling;