C₁₈H₂₀O₂Si

Base Information

Chemical Name:C₁₈H₂₀O₂Si
CAS No.:1558028-37-7
Molecular Formula:C₁₈H₂₀O₂Si
Molecular Weight:296.441
Hs Code.:

C<sub>18</sub>H<sub>20</sub>O<sub>2</sub>Si

Synonyms:C₁₈H₂₀O₂Si

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Chemical Property of C₁₈H₂₀O₂Si

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Technology Process of C₁₈H₂₀O₂Si

There total 7 articles about C₁₈H₂₀O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 4885-02-3
Dichloromethyl methyl ether

: 1558028-54-8
C₁₇H₁₈OSi

: 1558028-37-7
C₁₈H₂₀O₂Si

Guidance literature:: C₁₇H₁₈OSi; With 9-bora-bicyclo[3.3.1]nonane; In hexane; for 2h; Reflux;

With dimethylsulfide borane complex; for 2h; Reflux;

Dichloromethyl methyl ether; Further stages;
DOI:10.1021/om401208y

Reference yield: 57.0%

: 1558028-54-8
C₁₇H₁₈OSi

: N-cinnamyl-3-methylpyridin-2-amine

: 1558028-37-7
C₁₈H₂₀O₂Si

Guidance literature:: (4-methoxyphenyl)(phenyl)divinylsilane; N-cinnamyl-3-methylpyridin-2-amine; With chlorobis(cyclooctene)rhodium(I) dimer; tricyclohexylphosphine; In 5,5-dimethyl-1,3-cyclohexadiene; at 130 ℃; for 48h; Inert atmosphere; Sealed tube;

With hydrogenchloride; water; In 5,5-dimethyl-1,3-cyclohexadiene; at 20 ℃; for 3h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.1c04183

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 1558028-37-7
C₁₈H₂₀O₂Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium / tetrahydrofuran

1.2: 17 h / 20 °C

2.1: tetrahydrofuran / 1 h / Reflux

3.1: 9-bora-bicyclo[3.3.1]nonane / hexane / 2 h / Reflux

3.2: 2 h / Reflux

With magnesium; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; hexane;
DOI:10.1021/om401208y