C₁₃H₁₉NO₂Se

Base Information

• Chemical Name: C₁₃H₁₉NO₂Se
• CAS No.: 1612188-26-7
• Molecular Formula: C₁₃H₁₉NO₂Se
• Molecular Weight: 300.259
• Mol file: 1612188-26-7.mol

Synonyms:C₁₃H₁₉NO₂Se

Chemical Property of C₁₃H₁₉NO₂Se

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₃H₁₉NO₂Se

There total 4 articles about C₁₃H₁₉NO₂Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C10H11O2Se(1-)*Na(1+) → C13H19NO2Se (1612188-26-7)

Guidance literature:

In ethanol; for 3h; Inert atmosphere;

DOI:10.1080/10426507.2013.844144

Reference yield:

C20H22O4Se2 (1612188-24-5) → C13H19NO2Se (1612188-26-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 2 h / Inert atmosphere

2: ethanol / 3 h / Inert atmosphere

With sodium tetrahydroborate; In ethanol;

DOI:10.1080/10426507.2013.844144

Reference yield:

α-bromoacetophenone (70-11-1) → C13H19NO2Se (1612188-26-7)

Guidance literature:

Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / toluene / 8 h / Inert atmosphere; Dean-Stark; Reflux

2: selenium; hydrazine hydrate; sodium hydroxide / N,N-dimethyl-formamide / 3.5 h / 90 - 100 °C / Inert atmosphere

3: sodium tetrahydroborate / ethanol / 2 h / Inert atmosphere

4: ethanol / 3 h / Inert atmosphere

With selenium; sodium tetrahydroborate; toluene-4-sulfonic acid; hydrazine hydrate; sodium hydroxide; In ethanol; N,N-dimethyl-formamide; toluene;

DOI:10.1080/10426507.2013.844144

upstream raw materials:

2-(bromomethyl)-2-phenyl-1,3-dioxolane

C₂₀H₂₂O₄Se₂

α-bromoacetophenone