Technology Process of C19H21F3N2O3S2
There total 3 articles about C19H21F3N2O3S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium tetrafluoroborate; 1,10-Phenanthroline; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium diacetate; acetic acid;
In
N,N-dimethyl acetamide;
at 100 ℃;
for 24h;
Inert atmosphere;
DOI:10.1021/ml500024s
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 6 h / 23 °C / Inert atmosphere
2: ethanol / 16 h / 23 °C / Inert atmosphere
3: palladium diacetate; 1,10-Phenanthroline; lithium tetrafluoroborate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; acetic acid / N,N-dimethyl acetamide / 24 h / 100 °C / Inert atmosphere
With
lithium tetrafluoroborate; 1,10-Phenanthroline; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium diacetate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
ethanol; dichloromethane; N,N-dimethyl acetamide;
DOI:10.1021/ml500024s
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ethanol / 16 h / 23 °C / Inert atmosphere
2: palladium diacetate; 1,10-Phenanthroline; lithium tetrafluoroborate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; acetic acid / N,N-dimethyl acetamide / 24 h / 100 °C / Inert atmosphere
With
lithium tetrafluoroborate; 1,10-Phenanthroline; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium diacetate; acetic acid;
In
ethanol; N,N-dimethyl acetamide;
DOI:10.1021/ml500024s
