3,9,12,15,21-pentatosyl-3,9,12,15,,21,27-hexaaza-6,18-dioxabicyclo<21.3.1>heptaicosa-1(27),23,25-triene

Base Information

Chemical Name:3,9,12,15,21-pentatosyl-3,9,12,15,,21,27-hexaaza-6,18-dioxabicyclo<21.3.1>heptaicosa-1(27),23,25-triene
CAS No.:100919-57-1
Molecular Formula:C₅₄H₆₆N₆O₁₂S₅
Molecular Weight:1151.48
Hs Code.:

Synonyms:3,9,12,15,21-pentatosyl-3,9,12,15,,21,27-hexaaza-6,18-dioxabicyclo<21.3.1>heptaicosa-1(27),23,25-triene

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Chemical Property of 3,9,12,15,21-pentatosyl-3,9,12,15,,21,27-hexaaza-6,18-dioxabicyclo<21.3.1>heptaicosa-1(27),23,25-triene

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Technology Process of 3,9,12,15,21-pentatosyl-3,9,12,15,,21,27-hexaaza-6,18-dioxabicyclo<21.3.1>heptaicosa-1(27),23,25-triene

There total 7 articles about 3,9,12,15,21-pentatosyl-3,9,12,15,,21,27-hexaaza-6,18-dioxabicyclo<21.3.1>heptaicosa-1(27),23,25-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 7703-74-4
2,6-bis-(bromomethyl)pyridine

: C₄₇H₅₉N₅O₁₂S₅^(2-)*2Na⁽¹⁺⁾

: 100919-57-1
3,9,12,15,21-pentatosyl-3,9,12,15,,21,27-hexaaza-6,18-dioxabicyclo<21.3.1>heptaicosa-1(27),23,25-triene

Guidance literature:: In N,N-dimethyl-formamide; at 75 ℃;
DOI:10.1039/c39850001129

Reference yield: 30.0%

: 112633-27-9
2,6-bis<(p-tosylamino)methyl>pyridine

: 110661-80-8
6,9,12-tris(p-tolylsulfonyl)-6,9,12-triaza-3,15-dioxaheptadecane-1,17-diyl bis(methanesulfonate)

: 100919-57-1
3,9,12,15,21-pentatosyl-3,9,12,15,,21,27-hexaaza-6,18-dioxabicyclo<21.3.1>heptaicosa-1(27),23,25-triene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 24h;
DOI:10.1002/hlca.19890720525

Reference yield:

: 34984-16-2
2,6-bis(aminomethyl)pyridine

: 100919-57-1
3,9,12,15,21-pentatosyl-3,9,12,15,,21,27-hexaaza-6,18-dioxabicyclo<21.3.1>heptaicosa-1(27),23,25-triene

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent

2: 30 percent / K₂CO₃ / dimethylformamide / 24 h / 90 °C

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1002/hlca.19890720525