1-methoxy-2-hydroxy-3-isopropyl-5-allylbenzene

Base Information

• Chemical Name: 1-methoxy-2-hydroxy-3-isopropyl-5-allylbenzene
• CAS No.: 83569-74-8
• Molecular Formula: C₁₃H₁₈O₂
• Molecular Weight: 206.285
• Mol file: 83569-74-8.mol

Synonyms:1-methoxy-2-hydroxy-3-isopropyl-5-allylbenzene

Chemical Property of 1-methoxy-2-hydroxy-3-isopropyl-5-allylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1-methoxy-2-hydroxy-3-isopropyl-5-allylbenzene

There total 3 articles about 1-methoxy-2-hydroxy-3-isopropyl-5-allylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-methoxy-2-allyloxy-3-isopropylbenzene (83569-73-7) → 1-methoxy-2-hydroxy-3-isopropyl-5-allylbenzene (83569-74-8)

Guidance literature:

In various solvent(s); for 16h; Heating;

DOI:10.1016/0040-4020(82)80219-6

Reference yield:

3-isopropylbenzene-1,2-diol (2138-48-9) → 1-methoxy-2-hydroxy-3-isopropyl-5-allylbenzene (83569-74-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 70 percent / K₂CO₃ / acetone / 1.5 h / Ambient temperature

2: 1.) NaH / 1.) benzene, reflux, 2 h; 2.) 3-pentanone, reflux, 2 h

3: 91 percent / various solvent(s) / 16 h / Heating

With sodium hydride; potassium carbonate; In acetone;

DOI:10.1016/0040-4020(82)80219-6

Reference yield:

1-methoxy-2-hydroxy-3-isopropylbenzene (21022-74-2) → 1-methoxy-2-hydroxy-3-isopropyl-5-allylbenzene (83569-74-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaH / 1.) benzene, reflux, 2 h; 2.) 3-pentanone, reflux, 2 h

2: 91 percent / various solvent(s) / 16 h / Heating

With sodium hydride; In various solvent(s);

DOI:10.1016/0040-4020(82)80219-6

upstream raw materials:

1-methoxy-2-allyloxy-3-isopropylbenzene

3-isopropylbenzene-1,2-diol

1-methoxy-2-hydroxy-3-isopropylbenzene

Downstream raw materials:

1,2-dimethoxy-3-isopropyl-5-allylbenzene

3-(3,4-dimethoxy-5-isopropylphenyl)propanol

3-(3,4-dimethoxy-5-isopropylphenyl)propanal

2-methyl-5-(3,4-dimethoxy-5-isopropylphenyl)-1-penten-3-ol