C₄₄H₃₆O₅S

Base Information

Chemical Name:C₄₄H₃₆O₅S
CAS No.:1027525-63-8
Molecular Formula:C₄₄H₃₆O₅S
Molecular Weight:676.833
Hs Code.:

C<sub>44</sub>H<sub>36</sub>O<sub>5</sub>S

Synonyms:C₄₄H₃₆O₅S

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Chemical Property of C₄₄H₃₆O₅S

Chemical Property:

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Technology Process of C₄₄H₃₆O₅S

There total 10 articles about C₄₄H₃₆O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96-32-2
bromoacetic acid methyl ester

: 250342-58-6
4,4''-dimethoxy-5'-{4-[2-(phenylmethyl)benzo[b]thien-3-yl]phenyl}-[1,1';3',1''-terphenyl]-2'-ol

: 1027525-63-8
C₄₄H₃₆O₅S

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 75 ℃; for 2h;
DOI:10.1021/jm990560c

Reference yield:

: 7342-82-7
3-Bromothianaphthene

: 1027525-63-8
C₄₄H₃₆O₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: 85 percent / Pd(OAc)2; aq. K₂CO₃ / acetone / 2 h / 65 °C

2.1: BBr₃ / CH₂Cl₂ / 10 h / 20 °C

3.1: n-BuLi / tetrahydrofuran / 3 h / -40 °C

3.2: tetrahydrofuran / 0.5 h / 0 °C

4.1: hydrazine monohydrate; diethylene glycol / 1 h / 180 °C

4.2: KOH / 10 h / 130 °C

5.1: Br₂; KOAc / acetic acid / 0.17 h / 5 °C

6.1: 41 percent / palladium(II) acetate; barium hydroxide / 1,2-dimethoxy-ethane; H₂O / 10 h / 75 °C

7.1: K₂CO₃ / dimethylformamide / 2 h / 75 °C

With palladium diacetate; barium dihydroxide; n-butyllithium; bromine; potassium acetate; palladium diacetate; boron tribromide; potassium carbonate; hydrazine hydrate; diethylene glycol; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; acetone; 1.1: Cyclization / 2.1: demethylation / 3.1: Metallation / 3.2: Acylation / 4.1: Wolff-Kishner reduction / 4.2: Wolff-Kishner reduction / 5.1: Bromination / 6.1: Substitution / 7.1: Alkylation;
DOI:10.1021/jm990560c

Reference yield:

: 100-68-5
methyl-phenyl-thioether

: 1027525-63-8
C₄₄H₃₆O₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-BuLi; tetramethylenediamine / diethyl ether / 12 h / 20 °C

1.2: 23 percent / diethyl ether / 20 h / 20 °C

2.1: BBr₃ / CH₂Cl₂ / 10 h / 20 °C

3.1: n-BuLi / tetrahydrofuran / 3 h / -40 °C

3.2: tetrahydrofuran / 0.5 h / 0 °C

4.1: hydrazine monohydrate; diethylene glycol / 1 h / 180 °C

4.2: KOH / 10 h / 130 °C

5.1: Br₂; KOAc / acetic acid / 0.17 h / 5 °C

6.1: 41 percent / palladium(II) acetate; barium hydroxide / 1,2-dimethoxy-ethane; H₂O / 10 h / 75 °C

7.1: K₂CO₃ / dimethylformamide / 2 h / 75 °C

With barium dihydroxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; bromine; potassium acetate; palladium diacetate; boron tribromide; potassium carbonate; hydrazine hydrate; diethylene glycol; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; 1.1: Metallation / 1.2: Cyclization / 2.1: demethylation / 3.1: Metallation / 3.2: Acylation / 4.1: Wolff-Kishner reduction / 4.2: Wolff-Kishner reduction / 5.1: Bromination / 6.1: Substitution / 7.1: Alkylation;
DOI:10.1021/jm990560c