Ir4(CO)8(μ-κ2-PPh2(o-C6H4)PPh)(μ3-PPh2(η1:η2-o-C6H4))

Base Information

Chemical Name:Ir4(CO)8(μ-κ2-PPh2(o-C6H4)PPh)(μ3-PPh2(η1:η2-o-C6H4))
CAS No.:700346-80-1
Molecular Formula:C₅₀H₃₃Ir₄O₈P₃
Molecular Weight:1623.61
Hs Code.:

Synonyms:Ir4(CO)8(μ-κ2-PPh2(o-C6H4)PPh)(μ3-PPh2(η1:η2-o-C6H4))

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Chemical Property of Ir4(CO)8(μ-κ2-PPh2(o-C6H4)PPh)(μ3-PPh2(η1:η2-o-C6H4))

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Technology Process of Ir4(CO)8(μ-κ2-PPh2(o-C6H4)PPh)(μ3-PPh2(η1:η2-o-C6H4))

There total 2 articles about Ir4(CO)8(μ-κ2-PPh2(o-C6H4)PPh)(μ3-PPh2(η1:η2-o-C6H4)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 19631-23-3
Ir₄(P(C₆H₅)3)3(CO)9

: 700346-80-1
Ir₄(CO)8(P(C₆H₅)2(C₆H₄)P(C₆H₅))(P(C₆H₅)2(C₆H₄))

Guidance literature:: In chlorobenzene; heating in refluxing chlorobenzene for 40 min at 132 °C; elem. anal.; Kinetics;
DOI:10.1002/anie.200353290

Reference yield: 64.0%

: 19631-23-3
Ir₄(P(C₆H₅)3)3(CO)9

: 700346-80-1
Ir4(CO)8(μ-κ2-PPh2(o-C6H4)PPh)(μ3-PPh2(η1:η2-o-C6H4))

Guidance literature:: In chlorobenzene; heating of soln. of Ir complex in C6H5Cl to reflux for 40 min under N2; evapn. of solvent, TLC (CH2Cl2/C6H14 = 1:1), elem. anal.;
DOI:10.1021/ja0616027