4-Methyl-3-(2-hydroxyethylamino)-4H-1,2,4-benzothiadiazin-1,1-dioxide

Base Information

Chemical Name:4-Methyl-3-(2-hydroxyethylamino)-4H-1,2,4-benzothiadiazin-1,1-dioxide
CAS No.:109902-09-2
Molecular Formula:C₁₀H₁₃N₃O₃S
Molecular Weight:255.298
Hs Code.:
Mol file:109902-09-2.mol

Synonyms:Ethanol,2-[(4-methyl-4H-1,2,4-benzothiadiazin-3-yl)amino]-, S,S-dioxide; 4H-1,2,4-Benzothiadiazine,ethanol deriv.; NSC 373860

Suppliers and Price of 4-Methyl-3-(2-hydroxyethylamino)-4H-1,2,4-benzothiadiazin-1,1-dioxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4-Methyl-3-(2-hydroxyethylamino)-4H-1,2,4-benzothiadiazin-1,1-dioxide 95+%
1g
$ 469.00

American Custom Chemicals Corporation
4-METHYL-3-(2-HYDROXYETHYLAMINO)-4H-1,2,4-BENZOTHIADIAZIN-1,1-DIOXIDE 95.00%
5MG
$ 501.19

Total 6 raw suppliers

Chemical Property of 4-Methyl-3-(2-hydroxyethylamino)-4H-1,2,4-benzothiadiazin-1,1-dioxide

Chemical Property:

Vapor Pressure:1.83E-09mmHg at 25°C
Refractive Index:1.659
Boiling Point:465.5°C at 760 mmHg
Flash Point:235.3°C
PSA：90.38000
Density:1.47g/cm³
LogP:0.73530

Purity/Quality:

97% ^*data from raw suppliers

4-Methyl-3-(2-hydroxyethylamino)-4H-1,2,4-benzothiadiazin-1,1-dioxide 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Methyl-3-(2-hydroxyethylamino)-4H-1,2,4-benzothiadiazin-1,1-dioxide

There total 1 articles about 4-Methyl-3-(2-hydroxyethylamino)-4H-1,2,4-benzothiadiazin-1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 107089-76-9
NSC 373853

: 141-43-5
ethanolamine

: 109902-09-2
3-(2-hydroxyethylamino)-4-methyl-2H-1,2,4-benzothiadiazine 1,1-dioxide

Guidance literature:: In 1,4-dioxane; for 4h; Heating;
DOI:10.1016/0223-5234(87)90012-2

Reference yield:

: 109902-09-2
3-(2-hydroxyethylamino)-4-methyl-2H-1,2,4-benzothiadiazine 1,1-dioxide

: 65998-85-8
2,10-dihydro-10-methyl-3H-imidazo<1,2-b><1,2,4>benzothiadiazine 5,5-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 15 deg C, 2 h, then r. t., overnight

2: aq. K₂CO₃ / ethanol / 0.25 h / Ambient temperature

With thionyl chloride; potassium carbonate; In ethanol;
DOI:10.1016/0223-5234(87)90012-2